Invention Grant
US08455693B2 Process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG)
有权
制备2-（2-叔丁基氨基乙氧基）乙醇（叔丁基氨基二甘醇，TBADG）
- Patent Title: Process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG)
- Patent Title (中): 制备2-（2-叔丁基氨基乙氧基）乙醇（叔丁基氨基二甘醇，TBADG）
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Application No.: US13112161Application Date: 2011-05-20
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Publication No.: US08455693B2Publication Date: 2013-06-04
- Inventor: Roland Bou Chedid , Johann-Peter Melder , Steven Brughmans , Torsten Katz
- Applicant: Roland Bou Chedid , Johann-Peter Melder , Steven Brughmans , Torsten Katz
- Applicant Address: DE
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE
- Agency: Novak Druce Connolly Bove + Quigg LLP
- Main IPC: C07C209/16
- IPC: C07C209/16
Abstract:
A process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG) by reacting diethylene glycol (DG) with tert-butylamine (TBA) in the presence of hydrogen and of a copper catalyst, by effecting the reaction at a temperature in the range from 160 to 220° C. in the presence of a copper- and aluminum oxide-containing catalyst, where the catalytically active material of the catalyst, before the reduction thereof with hydrogen, comprises 20 to 75% by weight of aluminum oxide (Al2O3), 20 to 75% by weight of oxygen compounds of copper, calculated as CuO, and ≦5% by weight of oxygen compounds of nickel, calculated as NiO.
Public/Granted literature
- US20110288337A1 PROCESS FOR PREPARING 2-(2-TERT-BUTYLAMINOETHOXY)ETHANOL (TERT-BUTYLAMINODIGLYCOL, TBADG) Public/Granted day:2011-11-24
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