Invention Grant
- Patent Title: Method for producing hydroxyalkyl (meth)acrylate
- Patent Title (中): (甲基)丙烯酸羟烷基酯的制备方法
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Application No.: US13055607Application Date: 2009-08-28
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Publication No.: US08461374B2Publication Date: 2013-06-11
- Inventor: Masanori Tokuda , Michiyuki Kouno , Junichi Morioka
- Applicant: Masanori Tokuda , Michiyuki Kouno , Junichi Morioka
- Applicant Address: JP Tokyo
- Assignee: Mitsubishi Rayon Co., Ltd.
- Current Assignee: Mitsubishi Rayon Co., Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: JP2008-219548 20080828
- International Application: PCT/JP2009/004241 WO 20090828
- International Announcement: WO2010/023953 WO 20100304
- Main IPC: C07C67/26
- IPC: C07C67/26

Abstract:
Disclosed is a method for producing a hydroxyalkyl (meth)acrylate having high production efficiency and placing little burden on a production system. The method for producing a hydroxyalkyl (meth)acrylate comprises a reaction step of reacting (meth)acrylic acid with an alkylene oxide in a reactor while stirring a liquid containing (meth)acrylic acid and the alkylene oxide with a stirrer to obtain a reaction liquid containing a hydroxyalkyl (meth)acrylate, and thereafter a deaeration step of reducing a pressure in the reactor while stirring the reaction liquid with the stirrer to vaporize and remove an unreacted alkylene oxide in the reaction liquid, a number of stirring revolutions of the stirrer in the deaeration step being reduced to 30 to 85% of a number of stirring revolutions of the stirrer in the reaction step.
Public/Granted literature
- US20110124906A1 METHOD FOR PRODUCING HYDROXYALKYL (METH)ACRYLATE Public/Granted day:2011-05-26
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