Invention Grant
- Patent Title: Process for the preparation of 4-sulfinyl-pyrazole derivatives
- Patent Title (中): 4-亚磺酰基 - 吡唑衍生物的制备方法
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Application No.: US13504574Application Date: 2010-10-26
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Publication No.: US08476459B2Publication Date: 2013-07-02
- Inventor: Alexander Korte , Paul Hornung
- Applicant: Alexander Korte , Paul Hornung
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Brinks Hofer Gilson & Lione
- Priority: EP09174558 20091030
- International Application: PCT/EP2010/066162 WO 20101026
- International Announcement: WO2011/051284 WO 20110505
- Main IPC: C07D231/44
- IPC: C07D231/44

Abstract:
The present invention relates to a novel process for the preparation of a compound of formula (I), wherein R1, R2, R3, R4 and R5 are each independently selected from hydrogen, halogen, C1-C4-alkyl, C1-C4-haloalkyl, C1-C4-alkoxy, C1-C4-haloalkoxy, nitro, cyano, and pentafluorothio; R6 is C1-C4-alkyl, or C1-C4-haloalkyl; by oxidation of a compound of formula (II) with an oxidation agent selected from trifluoroperacetic acid and trichloroperacetic acid in the presence of a catalyst selected from hydroxides, oxides, sulfates, acetates or trifluoroacetates of lithium, magnesium, calcium, strontium, barium, titanium (IV), zinc (II) and manganese (II).
Public/Granted literature
- US20120215008A1 Process for the Preparation of 4-Sulfinyl-Pyrazole Derivatives Public/Granted day:2012-08-23
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