Invention Grant
- Patent Title: Process for preparing isocyanates in the gas phase
- Patent Title (中): 在气相中制备异氰酸酯的方法
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Application No.: US13035166Application Date: 2011-02-25
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Publication No.: US08487127B2Publication Date: 2013-07-16
- Inventor: Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
- Applicant: Torsten Mattke , Ralf Boehling , Carsten Knoesche , Vanessa Simone Lehr
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Main IPC: C07C263/10
- IPC: C07C263/10

Abstract:
The invention relates to a process for preparing isocyanates by reacting the corresponding amines with phosgene in the gas phase, in the presence or absence of an inert medium, which comprises the following steps: (a) vaporization of the amine in a vaporizer, (b) superheating of the amine, (c) mixing of the gaseous amine with the phosgene and introduction into a reaction zone, (d) reaction of amine and phosgene to give isocyanate in the reaction zone, with a reaction mixture comprising isocyanate and hydrogen chloride being formed, (e) cooling of the reaction mixture comprising isocyanate and hydrogen chloride, wherein the vaporizer comprises a vessel in which tubes through which a heating medium flows are comprised, where number and diameter of the tubes are designed so that the tubes have a specific heat transfer area based on the volume through which the amine flows of at least 300 m2/m3.
Public/Granted literature
- US20110213177A1 PROCESS FOR PREPARING ISOCYANATES IN THE GAS PHASE Public/Granted day:2011-09-01
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