Invention Grant
- Patent Title: Method of making pure salt from frac-water/wastewater
- Patent Title (中): 从压裂水/废水中制造纯盐的方法
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Application No.: US13421147Application Date: 2012-03-15
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Publication No.: US08529155B2Publication Date: 2013-09-10
- Inventor: Frank A. DiTommaso , Peter N. DiTommaso
- Applicant: Frank A. DiTommaso , Peter N. DiTommaso
- Applicant Address: US DE Dover
- Assignee: FracPure Holdings LLC
- Current Assignee: FracPure Holdings LLC
- Current Assignee Address: US DE Dover
- Agency: Lerner, David, Littenberg, Krumholz & Mentlik, LLP
- Main IPC: C02F1/00
- IPC: C02F1/00 ; C01F11/24 ; C01D3/04 ; B09B3/00

Abstract:
The present invention relates to a method for making pure salt comprises recapturing post-drilling flowback water from hydro-fracturing; removing oil from the flowback water; filtering the flowback water using an ultra filter with a pore size of about 0.1 microns or less to remove solid particulates and large organic molecules, such as benzene, ethylbenzene, toluene, and xylene, from the water; concentrating the flowback water to produce a brine that contains from about 15 wt % to about 40 wt % of salt relative to the total weight of the flowback brine; performing one or more chemical precipitation process using an effective amount of reagents to precipitate out the desired high quality commercial products, such as, barium sulfate, strontium carbonate, calcium carbonate; and crystallizing the chemically treated and concentrated flowback brine to produce greater than 99.5% pure salt products, such as sodium and calcium chloride.
Public/Granted literature
- US20120168157A1 METHOD OF MAKING PURE SALT FROM FRAC-WATER/WASTEWATER Public/Granted day:2012-07-05
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