Invention Grant
- Patent Title: Method for reducing the formation of by-product dinitrobenzene in the production of mononitrobenzene
- Patent Title (中): 减少副产物二硝基苯在单硝基苯生产中形成的方法
-
Application No.: US13129023Application Date: 2008-11-14
-
Publication No.: US08604256B2Publication Date: 2013-12-10
- Inventor: Sergio Berretta , David A. Boyd
- Applicant: Sergio Berretta , David A. Boyd
- Applicant Address: IE Dublin
- Assignee: Noram International Limited
- Current Assignee: Noram International Limited
- Current Assignee Address: IE Dublin
- Agency: McKee, Voorhees & Sease, P.L.C.
- International Application: PCT/CA2008/001996 WO 20081114
- International Announcement: WO2010/054462 WO 20100520
- Main IPC: C07C205/00
- IPC: C07C205/00

Abstract:
A method for making mononitrobenzene using a plug flow reactor train. Benzene, nitric acid and sulfuric acid are introduced into the reactor and produced mononitrobenzene is removed at an outlet end. All of the benzene and at least part of the sulfuric acid are introduced at the inlet end of the reactor. A first portion of the nitric acid is introduced by a first nitric acid feed into the inlet end and a second portion of the nitric acid is introduced at one or more additional feeds that are spaced between the inlet end and the outlet end. The method results in reduced formation of by-product dinitrobenzene, improving the reaction yield of mononitrobenzene while avoiding the need for a distillation step.
Public/Granted literature
- US20110218368A1 METHOD FOR REDUCING THE FORMATION OF BY-PRODUCT DINITROBENZENE IN THE PRODUCTION OF MONONITROBENZENE Public/Granted day:2011-09-08
Information query