Invention Grant
US08623309B2 Methods of preparing clusterboron 有权
聚集体硼的制备方法

  • Patent Title: Methods of preparing clusterboron
  • Patent Title (中): 聚集体硼的制备方法
  • Application No.: US12741198
    Application Date: 2008-11-03
  • Publication No.: US08623309B2
    Publication Date: 2014-01-07
  • Inventor: Kevin S. Cook
  • Applicant: Kevin S. Cook
  • Applicant Address: US MA North Billerica
  • Assignee: SemEquip, Inc.
  • Current Assignee: SemEquip, Inc.
  • Current Assignee Address: US MA North Billerica
  • Agency: Edwards Wildman Palmer LLP
  • Agent Peter F. Corless
  • International Application: PCT/US2008/012469 WO 20081103
  • International Announcement: WO2009/058405 WO 20090507
  • Main IPC: C01B6/10
  • IPC: C01B6/10
Methods of preparing clusterboron
Abstract:
The invention provides new methods for synthesis of ClusterBoron (B18H22). Preferred methods of the invention include in situ generation of the conjugate acid of B20H182− and degradation of the acid in solution to produce B18H22 in high yields and high purity. The invention further provides isotopically enriched boranes, particularly isotopically enriched 10B)18H22 and 11B18H22.
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