Invention Grant
- Patent Title: Process for preparing a cyclic tertiary methylamine
- Patent Title (中): 制备环状叔甲胺的方法
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Application No.: US13158667Application Date: 2011-06-13
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Publication No.: US08637668B2Publication Date: 2014-01-28
- Inventor: Christof Wilhelm Wigbers , Johann-Peter Melder , Bernd Stein , Harald Meiβner
- Applicant: Christof Wilhelm Wigbers , Johann-Peter Melder , Bernd Stein , Harald Meiβner
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Novak Druce Connolly Bove + Quigg LLP
- Main IPC: C07D295/03
- IPC: C07D295/03

Abstract:
Process for preparing a cyclic tertiary methylamine of the formula I where A is a C4-alkylene group, a C5-alkylene group or a —(CH2)2—B—(CH2)2— group, where B is oxygen (O) or an N—R1 radical and R1 is C1-C5-alkyl, aryl or C5-C7-cycloalkyl, wherein an amino alcohol II from the group consisting of 1,4-aminobutanol, 1,5-aminopentanol, aminodiglycol (ADG) or aminoethylethanolamine of the formula IIa where R1 is as defined above or is hydrogen (H), in which case R1═CH3 in the amine I, is reacted with methanol in a reactor at a temperature in the range from 150 to 270° C. in the liquid phase in the presence of a copper-comprising heterogeneous catalyst.
Public/Granted literature
- US20120157679A1 PROCESS FOR PREPARING A CYCLIC TERTIARY METHYLAMINE Public/Granted day:2012-06-21
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