Invention Grant
US08653232B2 Manufacturing method of polyethylene terephthalate 有权
聚对苯二甲酸乙二醇酯的制造方法

  • Patent Title: Manufacturing method of polyethylene terephthalate
  • Patent Title (中): 聚对苯二甲酸乙二醇酯的制造方法
  • Application No.: US12295211
    Application Date: 2007-04-05
  • Publication No.: US08653232B2
    Publication Date: 2014-02-18
  • Inventor: Shinya Konuma
  • Applicant: Shinya Konuma
  • Applicant Address: JP Osaka
  • Assignee: Teijin Fibers Limited
  • Current Assignee: Teijin Fibers Limited
  • Current Assignee Address: JP Osaka
  • Agency: Sughrue Mion, PLLC
  • Priority: JP2006-105087 20060406; JP2006-272854 20061004
  • International Application: PCT/JP2007/058016 WO 20070405
  • International Announcement: WO2007/117028 WO 20071018
  • Main IPC: C08G63/91
  • IPC: C08G63/91 C08F6/26
Manufacturing method of polyethylene terephthalate
Abstract:
A manufacturing method of polyethylene terephthalate including a step of melt polycondensation in presence of polycondensation catalyst represented by general Formula (I), wherein R1 represents an alkyl group having from 2 to 12 carbon atoms, and melt polycondensed polyethylene terephthalate has an intrinsic viscosity of from 0.48 to 0.53 dL/g and a terminal carboxyl number of from 14 to 22 mmol/kg; and a step of solid phase polycondensation to obtain solid phase polycondensed polyethylene terephthalate having an intrinsic viscosity of from 0.70 to 0.86 dL/g, and a terminal carboxyl number of less than 15 mmol/kg, followed by a step of applying an aqueous solution of at least one salt selected from the group consisting of acetate, carbonate, and sulfate of sodium, potassium, or cesium to the solid phase polycondensed polyethylene terephthalate, and then drying the polyethylene terephthalate, wherein the final content of sodium, potassium or cesium atom in dried polyethylene terephthalate is from 2 to 25 ppm.
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