Invention Grant
US08658810B2 Method for producing purified dialkyl-furan-2,5-dicarboxylate vapor
有权
纯化的二烷基 - 呋喃-2,5-二羧酸二烷基酯蒸气的生产方法
- Patent Title: Method for producing purified dialkyl-furan-2,5-dicarboxylate vapor
- Patent Title (中): 纯化的二烷基 - 呋喃-2,5-二羧酸二烷基酯蒸气的生产方法
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Application No.: US13530738Application Date: 2012-06-22
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Publication No.: US08658810B2Publication Date: 2014-02-25
- Inventor: Lee Reynolds Partin , Ashfaq Shaikh , Mesfin Ejerssa Janka , Kenny Randolph Parker
- Applicant: Lee Reynolds Partin , Ashfaq Shaikh , Mesfin Ejerssa Janka , Kenny Randolph Parker
- Applicant Address: US TN Kingsport
- Assignee: Eastman Chemical Company
- Current Assignee: Eastman Chemical Company
- Current Assignee Address: US TN Kingsport
- Agent Dennis V. Carmen; Steven A. Owen
- Main IPC: C07D307/02
- IPC: C07D307/02

Abstract:
Disclosed is a process to produce a purified vapor comprising dialkyl-furan-2,5-dicarboxylate (DAFD). Furan-2,5-dicarboxylic acid (FDCA) and an alcohol in an esterification zone to generate a crude diester stream containing dialkyl furan dicarboxylate (DAFD), unreacted alcohol, 5-(alkoxycarbonyl)furan-2-carboxylic acid (ACFC), and alkyl furan-2-carboxylate (AFC). The crude diester stream is fed to a flash evaporation zone to produce a vapor alcohol composition and a first liquid DAFD rich composition. At least a portion of the remaining alcohol can be separated from the first liquid DAFD rich composition to produce a second alcohol vapor and a second liquid DAFD rich composition, followed by separating AFC from the second liquid DAFD rich composition to product an AFC vapor and a partially purified DAFD rich composition, followed by separating a portion of the DAFD from the partially purified DAFD rich composition to produce a purified DAFD vapor.
Public/Granted literature
- US20130345447A1 METHOD FOR PRODUCING PURIFIED DIALKYL-FURAN-2,5-DICARBOXYLATE VAPOR Public/Granted day:2013-12-26
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