Invention Grant
- Patent Title: Method of manufacturing silicon single crystal, apparatus for pulling silicon single crystal and vitreous silica crucible
- Patent Title (中): 硅单晶的制造方法,硅单晶拉丝装置和玻璃状石英坩埚
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Application No.: US12786911Application Date: 2010-05-25
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Publication No.: US08696813B2Publication Date: 2014-04-15
- Inventor: Masanori Fukui , Hideki Watanabe , Nobumitsu Takase
- Applicant: Masanori Fukui , Hideki Watanabe , Nobumitsu Takase
- Applicant Address: JP Akita
- Assignee: Japan Super Quartz Corporation
- Current Assignee: Japan Super Quartz Corporation
- Current Assignee Address: JP Akita
- Agency: Greenblum & Bernstein, P.L.C.
- Priority: JP2009-128291 20090527
- Main IPC: C30B15/04
- IPC: C30B15/04

Abstract:
Leakage of silicon melt is monitored and touch of a seed crystal at the silicon melt is detected, and in addition, reinforcement of a vitreous silica crucible to be endurable during pulling for a long time and decrease of impurity concentration of a silicon single crystal can be expected. A method for manufacturing a silicon single crystal is provided. The method includes: detecting touching status of a seed crystal at silicon melt by supplying voltage V1 using a crucible side as a negative electrode and a wire side as a positive electrode and by monitoring change of the voltage, when the seed crystal provided at a front end of the wire touches the silicon melt inside a vitreous silica crucible; devitrifying an inner surface of the vitreous silica crucible as supplying voltage V2 using the crucible side as a positive electrode and the wire side as a negative electrode during a temperature control period; and growing a silicon single crystal by slowly pulling the seed crystal as supplying voltage V3 using the crucible side as a negative electrode and the wire side as a positive electrode after the temperature control period.
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