Invention Grant
US08703997B2 Process for preparation and preferably distillative workup of diphenylmethane diisocyanate (MDI)
有权
二苯甲烷二异氰酸酯(MDI)的制备方法,优选蒸馏处理方法
- Patent Title: Process for preparation and preferably distillative workup of diphenylmethane diisocyanate (MDI)
- Patent Title (中): 二苯甲烷二异氰酸酯(MDI)的制备方法,优选蒸馏处理方法
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Application No.: US13393088Application Date: 2010-10-20
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Publication No.: US08703997B2Publication Date: 2014-04-22
- Inventor: Christian Schneider , Nikolaus Zafred , Andreas Heussler , Leo Denissen , Lucia Koenigsmann
- Applicant: Christian Schneider , Nikolaus Zafred , Andreas Heussler , Leo Denissen , Lucia Koenigsmann
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: EP09173515 20091020
- International Application: PCT/EP2010/065782 WO 20101020
- International Announcement: WO2011/048134 WO 20110428
- Main IPC: C07C263/00
- IPC: C07C263/00

Abstract:
What is proposed is a process for preparation and distillative workup of diphenylmethane diisocyanate (MDI), proceeding from a benzene-comprising feedstream, in which, in a catalytic hydrogenation of nitrobenzene to aniline, steam is raised at two different pressure levels, which partly or completely covers the energy demand for the overall process, by using two fluidized bed reactors of identical design, of which a first fluidized bed reactor is operated with an aniline load for which the fluidized bed reactors have been designed and provides steam at a first, lower pressure level, and a second fluidized bed reactor is operated with a load lowered with respect to the first fluidized bed reactor to such an extent that the second fluidized bed reactor affords steam at the higher pressure level.
Public/Granted literature
- US20120157709A1 PROCESS FOR PREPARATION AND PREFERABLY DISTILLATIVE WORKUP OF DIPHENYLMETHANE DIISOCYANATE (MDI) Public/Granted day:2012-06-21
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