Invention Grant
- Patent Title: Process for producing xylylenediamine
- Patent Title (中): 生产苯二甲胺的方法
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Application No.: US13062334Application Date: 2009-08-27
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Publication No.: US08759588B2Publication Date: 2014-06-24
- Inventor: Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
- Applicant: Shinichi Nagao , Tatsuyuki Kumano , Kenji Nakaya , Ryusuke Shigematsu , Kinji Kato
- Applicant Address: JP Tokyo
- Assignee: Mitsubishi Gas Chemical Company, Inc.
- Current Assignee: Mitsubishi Gas Chemical Company, Inc.
- Current Assignee Address: JP Tokyo
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: JP2008-230164 20080908
- International Application: PCT/JP2009/064989 WO 20090827
- International Announcement: WO2010/026920 WO 20100311
- Main IPC: C07C209/00
- IPC: C07C209/00

Abstract:
The invention provides a process for producing xylylenediamine, including supplying a solution of phthalonitrile dissolved in a solvent to a reactor filled with a catalyst and hydrogenating the phthalonitrile to produce xylylenediamine, characterized in that the process includes halting supply of the solution; (2) bringing a washing liquid into contact with the catalyst, the washing liquid having a phthalonitrile content of 3 mass % or less and a xylylenediamine content of 1 mass % or more; and after completion of the contact, resuming supply of the solution, and employing the catalyst continuously in hydrogenation. Through the production process of the invention, the catalyst can be employed continuously for a long period of time, and the catalyst-related cost can be considerably reduced.
Public/Granted literature
- US20110245540A1 PROCESS FOR PRODUCING XYLYLENEDIAMINE Public/Granted day:2011-10-06
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