Invention Grant
- Patent Title: Production method of titanium oxide sol
- Patent Title (中): 氧化钛溶胶的制备方法
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Application No.: US13128496Application Date: 2009-10-27
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Publication No.: US08802159B2Publication Date: 2014-08-12
- Inventor: Hirokazu Kato , Natsumi Tsuihiji
- Applicant: Hirokazu Kato , Natsumi Tsuihiji
- Applicant Address: JP Tokyo
- Assignee: Nissan Chemical Industries, Ltd.
- Current Assignee: Nissan Chemical Industries, Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Oliff PLC
- Priority: JP2008-289452 20081112
- International Application: PCT/JP2009/068398 WO 20091027
- International Announcement: WO2010/055770 WO 20100520
- Main IPC: A01N59/16
- IPC: A01N59/16 ; B01J21/06 ; H01B1/02 ; A01P1/00 ; C01G23/053 ; B01J13/00 ; C09C1/36

Abstract:
There is provided a method for efficiently producing an anatase-type titanium oxide sol in an extremely advantageous dispersion state. The method comprises mixing a titanium alkoxide, an organic acid, and a quaternary ammonium hydroxide with water in a molar ratio of the organic acid of 0.4 to 4.0 relative to 1 mol of a titanium atom of the titanium alkoxide and in a molar ratio of the quaternary ammonium hydroxide of 0.8 to 1.9 relative to 1 mol of the organic acid to prepare an aqueous mixed solution having a concentration in terms of TiO2 of 0.5 to 10% by mass; heating the aqueous mixed solution to 50 to 100° C. to remove an alcohol; and subjecting the resulting titanium-containing aqueous solution to a hydrothermal treatment at 110 to 170° C.
Public/Granted literature
- US20110274767A1 PRODUCTION METHOD OF TITANIUM OXIDE SOL Public/Granted day:2011-11-10
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