Invention Grant
- Patent Title: Method for producing a free acid from the salt thereof
- Patent Title (中): 从其盐生产游离酸的方法
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Application No.: US13141456Application Date: 2010-02-01
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Publication No.: US08809576B2Publication Date: 2014-08-19
- Inventor: Alexander Schraven , Thomas Tacke , Thomas Haas , Christoph Kobler , Dieter Buss , Axel Ronneburg , Olivier Zehnacker
- Applicant: Alexander Schraven , Thomas Tacke , Thomas Haas , Christoph Kobler , Dieter Buss , Axel Ronneburg , Olivier Zehnacker
- Applicant Address: DE Essen
- Assignee: Evonik Degussa GmbH
- Current Assignee: Evonik Degussa GmbH
- Current Assignee Address: DE Essen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: DE102009009580 20090219
- International Application: PCT/EP2010/051170 WO 20100201
- International Announcement: WO2010/094554 WO 20100826
- Main IPC: C07F9/22
- IPC: C07F9/22

Abstract:
The invention relates to an improved method for releasing an organic acid, preferably a carbon, sulfone or phosphone acid, particularly an alpha or beta hydroxycarbon acid, from the ammonia salt thereof by releasing and removing ammoniac and simultaneous extraction of the released acid, having an amine as a suitable extraction means from the aqueous phase. This method corresponds to a reactive extraction. The reactive extraction of an organic acid from the aqueous ammonia salt solution thereof can be significantly improved by the use of a strip medium or carrier gas, such as nitrogen, air, water vapor or inert gases such as argon. The released ammoniac is removed from the aqueous solution by the continuous gas flow and can be resupplied into a production process. The free acid can be obtained by a method such as distillation, rectification, crystallization, reextraction, chromatography, adsorption or by a membrane method from the extraction means.
Public/Granted literature
- US20110257429A1 METHOD FOR PRODUCING A FREE ACID FROM THE SALT THEREOF Public/Granted day:2011-10-20
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