Invention Grant
US08816125B2 Process for the continuous preparation of (cyclo)aliphatic diisocyanates 有权
连续制备(环)脂族二异氰酸酯的方法

Process for the continuous preparation of (cyclo)aliphatic diisocyanates
Abstract:
The invention relates to a multi-stage process for the continuous, phosgene-free preparation of (cyclo)aliphatic diisocyanates that comprises the conversion of (cyclo)aliphatic diamines into the corresponding (cyclo)alkylene biscarbamates and the thermal cleaving of the latter into the (cyclo)alkylene diisocyanates and alcohol. The urea used in accordance with the invention and also the urea employed for the preparation of urea equivalents (e.g. alkyl carbonates, alkyl carbamates) as a possible precursor for the synthesis of the (cyclo)aliphatic biscarbamates is unconditioned.
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