Invention Grant
US08829245B2 3-aminomethyl-3, 5, 5-trimethyl cyclohexylamine preparation method
有权
3-氨基甲基-3,5,5-三甲基环己胺制备方法
- Patent Title: 3-aminomethyl-3, 5, 5-trimethyl cyclohexylamine preparation method
- Patent Title (中): 3-氨基甲基-3,5,5-三甲基环己胺制备方法
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Application No.: US14113907Application Date: 2011-09-06
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Publication No.: US08829245B2Publication Date: 2014-09-09
- Inventor: Changsheng Chen , Yuan Li , Wenjuan Zhao , Hongyin Cui , Weiqi Hua
- Applicant: Changsheng Chen , Yuan Li , Wenjuan Zhao , Hongyin Cui , Weiqi Hua
- Applicant Address: CN Yantai, Shandong CN Ningbo, Zhejiang
- Assignee: Wanhua Chemical Group Co., Ltd.,Wanhua Chemical (Ningbo) Co., Ltd.
- Current Assignee: Wanhua Chemical Group Co., Ltd.,Wanhua Chemical (Ningbo) Co., Ltd.
- Current Assignee Address: CN Yantai, Shandong CN Ningbo, Zhejiang
- Agency: Armstrong Teasdale LLP
- Priority: CN201110231786 20110808
- International Application: PCT/CN2011/079372 WO 20110906
- International Announcement: WO2013/020316 WO 20130214
- Main IPC: C07C209/48
- IPC: C07C209/48 ; C07C209/62 ; C07C211/36

Abstract:
Provided is a 3-aminomethyl-3,5,5-trimethylcyclohexylamine preparation method. A feeding flow of 3-cyano-3,5,5-trimethylcyclohexylamine is reacted with NH3 and hydrogen in the presence of a hydrogenation catalyst; the method is characterized by: firstly adding a basic compound to the feeding flow of 3-cyano-3,5,5-trimethylcyclohexylamine, and then after a portion of 3-cyano-3,5,5-trimethylcyclohexylamine has reacted, adding an acidic compound to reaction materials for further hydrogenation reaction to prepare the product. The method ensures that the aminonitrile content in the product is low, thus effectively reducing the duration of the reaction and greatly reducing the consumption of the catalyst during the hydrogenation reaction process.
Public/Granted literature
- US20140142341A1 3-AMINOMETHYL-3, 5, 5-TRIMETHYL CYCLOHEXYLAMINE PREPARATION METHOD Public/Granted day:2014-05-22
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