Invention Grant
US08901186B2 Process for producing silica-comprising dispersions comprising polyetherols or polyether amines
有权
用于生产包含聚醚醚或聚醚胺的含二氧化硅的分散体的方法
- Patent Title: Process for producing silica-comprising dispersions comprising polyetherols or polyether amines
- Patent Title (中): 用于生产包含聚醚醚或聚醚胺的含二氧化硅的分散体的方法
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Application No.: US13203634Application Date: 2010-03-11
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Publication No.: US08901186B2Publication Date: 2014-12-02
- Inventor: Berend Eling , Zeljko Tomovic , Stefan Auffarth
- Applicant: Berend Eling , Zeljko Tomovic , Stefan Auffarth
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, Spivak, McClelland, Maier & Neustadt, L.L.P.
- Priority: EP09155131 20090313
- International Application: PCT/EP2010/053106 WO 20100311
- International Announcement: WO2010/103072 WO 20100916
- Main IPC: C08K3/36
- IPC: C08K3/36 ; C01B33/143 ; C01B33/145 ; C01B33/146 ; C01B33/148

Abstract:
Process for producing silica-comprising dispersions comprising a polyetherol or a polyether amine, which comprises the steps of (i) admixing an aqueous silica sol (K) having an average particle diameter of from 1 to 150 nm and a silica content, calculated as SiO2, of from 1 to 60% by weight and a pH of from 1 to 6 with at least one polyetherol (b1) and/or polyether amine (b2) based on ethylene oxide and/or propylene oxide and having an average OH or amine functionality of from 2 to 6 and a number average molecular weight of from 62 to 6000 g/mol, (ii) distilling off at least part of the water, (iii) admixing the dispersion with at least one compound (S) having at least one at least monoalkoxylated silyl group and at least one alkyl, cycloalkyl or aryl substituent, where this substituent may have groups which are reactive toward an alcohol, an amine or an isocyanate in an amount of from 0.1 to 20 μmol of (S) per m2 of surface area of (K), where steps (i) and (iii) can be carried out simultaneously or in succession in any order, (iv) optionally adjusting the pH of the silica-comprising dispersions obtained to a value of from 7 to 12 by adding a basic compound, where step (iv) can also be carried out between steps (ii) and (iii).
Public/Granted literature
- US20110313070A1 PROCESS FOR PRODUCING SILICA-COMPRISING DISPERSIONS COMPRISING POLYETHEROLS OR POLYETHER AMINES Public/Granted day:2011-12-22
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