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US08901292B2 Method of mass production of tetrakis(p-nitrophenyl)porphyrins 有权
大量生产四(对硝基苯基)卟啉的方法

Method of mass production of tetrakis(p-nitrophenyl)porphyrins
Abstract:
A method of mass production of tetrakis(p-nitrophenyl)porphyrins, by which successful isolation of the barely soluble product from meso-aryl nitration of tetraphenylporphyrin toward a remarkable yield of nearly 90% has been realized by means of a solid phase extraction technique. This is a simpler and more straight forward synthetic method, suitable production at an industrial scale with lower cost, shorter synthetic time and lower solvent consumption. A preferred species of tetrakis(p-nitrophenyl)porphyrin produced by a subject method is:
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