Invention Grant
- Patent Title: Polyisobutylene prepared at high velocity and circulation rate
- Patent Title (中): 聚异丁烯以高速度和循环速率制备
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Application No.: US14346367Application Date: 2012-10-10
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Publication No.: US08946361B2Publication Date: 2015-02-03
- Inventor: Sohel K. Shaikh , Alfred Chiu , Patrick L. Bradley , Gilbert D. Valdez , Peggy J. Macatangay
- Applicant: TPC Group LLC
- Applicant Address: US TX Houston
- Assignee: TPC Group LLC
- Current Assignee: TPC Group LLC
- Current Assignee Address: US TX Houston
- Agent Michael W. Ferrell
- International Application: PCT/US2012/059464 WO 20121010
- International Announcement: WO2013/062758 WO 20130502
- Main IPC: C08F2/00
- IPC: C08F2/00 ; C08F2/02 ; C08F2/14 ; B01J8/00 ; C08F2/01 ; C08F10/10 ; C08F110/10

Abstract:
A method of making a polyisobutylene polymer in a recirculating loop reactor with one or more reaction tubes in contact with a heat transfer medium includes controlling the delta P and polymerization reaction to provide a linear velocity of the reaction mixture of at least 11 ft/sec in the one or more tubes of the loop reactor and/or controlling the delta P and polymerization reaction of steps (b) and (c) to provide a recirculation ratio of the recirculation rate to the feed rate of at least 30:1. Typically, the process utilizes a recirculating pump operating at a at a pressure differential of from 35 psi to 70 psi.
Public/Granted literature
- US20140235801A1 Polyisobutylene Prepared at High Velocity and Circulation Rate Public/Granted day:2014-08-21
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