Invention Grant
- Patent Title: Purifying crude furan 2,5-dicarboxylic acid by hydrogenation
- Patent Title (中): 通过氢化纯化粗呋喃2,5-二羧酸
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Application No.: US13758080Application Date: 2013-02-04
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Publication No.: US08969404B2Publication Date: 2015-03-03
- Inventor: Mesfin Ejerssa Janka , Charles Edwan Sumner, Jr. , Shane Kipley Kirk , Ashfaq Shahanawaz Shaikh , Kenny Randolph Parker
- Applicant: Eastman Chemical Company
- Applicant Address: US TN Kingsport
- Assignee: Eastman Chemical Company
- Current Assignee: Eastman Chemical Company
- Current Assignee Address: US TN Kingsport
- Agent Dennis V. Carmen
- Main IPC: A61K31/341
- IPC: A61K31/341 ; C07D307/34 ; C07D307/68

Abstract:
A process for purifying a crude furan 2,5-dicarboxylic acid composition (cFDCA) by hydrogenation of a FDCA composition dissolved in a hydrogenation solvent such as water, and hydrogenating under mild conditions, such as at a temperature within a range of 130° C. to 225° C. by contacting the solvated FDCA composition with hydrogen in the presence of a hydrogenation catalyst under a hydrogen partial pressure within a range of 10 psi to 900 psi. A product FDCA composition is produced having a low amount of tetrahydrofuran dicarboxylic acid, a low b*, and a low amount of 5-formyl furan-2-carboxylic acid (FFCA).
Public/Granted literature
- US20130345452A1 PURIFYING CRUDE FURAN 2,5-DICARBOXYLIC ACID BY HYDROGENATION Public/Granted day:2013-12-26
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