Invention Grant
- Patent Title: Method for producing rutile type titanium oxide sol
- Patent Title (中): 金红石型氧化钛溶胶的制备方法
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Application No.: US14359393Application Date: 2012-11-30
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Publication No.: US09023147B2Publication Date: 2015-05-05
- Inventor: Natsumi Murakami , Ai Miyamoto , Yoshinari Koyama
- Applicant: Nissan Chemical Industries, Ltd.
- Applicant Address: JP Tokyo
- Assignee: Nissan Chemical Industries, Ltd.
- Current Assignee: Nissan Chemical Industries, Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Oliff PLC
- Priority: JP2011-264664 20111202
- International Application: PCT/JP2012/081176 WO 20121130
- International Announcement: WO2013/081136 WO 20130606
- Main IPC: C01G23/053
- IPC: C01G23/053 ; B82Y30/00 ; A01N25/08 ; B01J31/38 ; C09D5/16 ; C09D7/12

Abstract:
There is provided provide a method for efficiently producing a rutile type titanium sol having a particle diameter based on dynamic light scattering method of 5 nm to 100 nm that is excellent in dispersibility. The method for producing a rutile type titanium oxide sol comprising: process (a): mixing metastannic acid, a titanium alkoxide, a quaternary ammonium hydroxide, oxalic acid, and water so as to contain 0.02 moles to 0.8 moles of tin atoms, 0.1 moles to 3.5 moles of the quaternary ammonium hydroxide, and 0.1 moles to 8.0 moles of the oxalic acid with respect to 1 mole of titanium atoms of the titanium alkoxide to prepare a titanium-containing aqueous solution with a concentration in terms of TiO2 of 0.1% by mass to 15% by mass; and process (b): subjecting the titanium-containing aqueous solution obtained in process (a) to a hydrothermal treatment at a temperature from 100° C. to 170° C.
Public/Granted literature
- US20140328889A1 METHOD FOR PRODUCING RUTILE TYPE TITANIUM OXIDE SOL Public/Granted day:2014-11-06
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