Invention Grant
- Patent Title: Process for the organotemplate-free synthetic production of a zeolitic material using recycled mother liquor
- Patent Title (中): 使用回收母液的沸石材料的无机无模板合成生产方法
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Application No.: US13606614Application Date: 2012-09-07
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Publication No.: US09028795B2Publication Date: 2015-05-12
- Inventor: Bilge Yilmaz , Ulrich Müller , Faruk Özkirim , Meike Pfaff , Mike Haas , Feng-Shou Xiao
- Applicant: Bilge Yilmaz , Ulrich Müller , Faruk Özkirim , Meike Pfaff , Mike Haas , Feng-Shou Xiao
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Servilla Whitney LLC
- Priority: WOPCT/CN2011/079502 20110909
- Main IPC: C01B39/46
- IPC: C01B39/46 ; C01B39/30 ; C01B39/02

Abstract:
The present invention relates to an organotemplate-free synthetic process for the production of a zeolitic material comprising YO2 and X2O3, wherein said process comprises the steps of (1) preparing a mixture comprising seed crystals, one or more sources for YO2, one or more sources for X2O3, and one or more solvents; (2) crystallizing the mixture obtained in step (1) to obtain a zeolitic material comprising YO2 and X2O3 as a crystallization product; wherein Y is a tetravalent element, and X is a trivalent element, and wherein at least a portion of the mother liquor obtained in step (2) is recycled to step (1) as a source for YO2, optionally after concentration of the mother liquor.
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