Invention Grant
US09096733B2 Process for producing coalesced rubber microparticles and their blends with epoxy resins
有权
制备聚合橡胶微粒及其与环氧树脂的共混物的方法
- Patent Title: Process for producing coalesced rubber microparticles and their blends with epoxy resins
- Patent Title (中): 制备聚合橡胶微粒及其与环氧树脂的共混物的方法
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Application No.: US14085383Application Date: 2013-11-20
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Publication No.: US09096733B2Publication Date: 2015-08-04
- Inventor: Soobum Choi , Lawrence Justice , James Eckler
- Applicant: ZEON CHEMICALS L.P.
- Applicant Address: US KY Louisville
- Assignee: ZEON CHEMICALS L.P.
- Current Assignee: ZEON CHEMICALS L.P.
- Current Assignee Address: US KY Louisville
- Agency: Westerman, Hattori, Daniels & Adrian, LLP
- Main IPC: C08C1/15
- IPC: C08C1/15 ; C08J3/12 ; C08J3/00

Abstract:
Coalesced rubber particles having an average particle size of 5-50 microns are produced by: (1) adding simultaneously to a latex of pre-crosslinked rubber particles a solvent and an electrolyte solution to form swollen rubber aggregation particles, wherein the solvent has a lower boiling point than water and a capacity of swelling the rubber by at least 10 wt %, and the electrolyte is a solution of at least one metal salt; (2) removing the solvent under atmospheric pressure or low vacuum and at temperature greater than 80° C. to coalesce the rubber into particles having an average particle size of 5-50 50 microns; (3) filtering and washing with methanol; and (4) filtering the washed particles to remove methanol. An epoxy resin is blended with the particles and residual methanol removed, to obtain a blend containing coalesced rubber particles having an average particle size of 5-50 microns in the blended state.
Public/Granted literature
- US20150141576A1 PROCESS FOR PRODUCING COALESCED RUBBER MICROPARTICLES AND THEIR BLENDS WITH EPOXY RESINS Public/Granted day:2015-05-21
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