Invention Grant
- Patent Title: Methyltin mercaptide derivative and method for preparing the same
- Patent Title (中): 硫醇甲基锡衍生物及其制备方法
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Application No.: US14270347Application Date: 2014-05-05
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Publication No.: US09120832B2Publication Date: 2015-09-01
- Inventor: Yinghui Guo , Laoyong Yan , Baoliang Zhao , Qiangshun Yi , Bing Wei , Xiangyan Li , Shu Chen , Fuliang Duan
- Applicant: Yunnan Tin Company Limited
- Applicant Address: CN Gejiu
- Assignee: YUNNAN TIN COMPANY LIMITED
- Current Assignee: YUNNAN TIN COMPANY LIMITED
- Current Assignee Address: CN Gejiu
- Agency: Matthias Scholl P.C.
- Agent Matthias Scholl
- Priority: CN201310208211 20130529
- Main IPC: C07F7/22
- IPC: C07F7/22

Abstract:
A compound represented by formula I or II and a method for preparing the same. The method includes: a) adding isooctyl mercaptopropionate to a reactor, adding dropwise an aqueous solution of methyltin chloride, stirring and allowing for a complete reaction, and adding aqueous ammonia, an aqueous solution of sodium hydroxide, an aqueous solution of sodium bicarbonate, an aqueous solution of sodium carbonate, or a solution of an organic base to regulate the pH value of a resulting mixture from a starting value of between 2 and 8 to an end value of between 6 and 10 for a primary stage of esterification; and b) allowing a product obtained from step a) to proceed to a secondary stage of the esterification, allowing the product to stand until phases are separated, collecting and washing an organic phase using deionized water, allowing a resulting mixture to stand until phases are separated.
Public/Granted literature
- US20140357883A1 METHYLTIN MERCAPTIDE DERIVATIVE AND METHOD FOR PREPARING THE SAME Public/Granted day:2014-12-04
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