Invention Grant
- Patent Title: Method for producing an aliphatic polyester having increased molecular weight
- Patent Title (中): 具有分子量增加的脂肪族聚酯的制造方法
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Application No.: US14353647Application Date: 2012-10-17
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Publication No.: US09175127B2Publication Date: 2015-11-03
- Inventor: Yasushi Ichikawa , Hideharu Kimura , Akira Ishii
- Applicant: SHOWA DENKO K.K.
- Applicant Address: JP Tokyo
- Assignee: SHOWA DENKO K.K.
- Current Assignee: SHOWA DENKO K.K.
- Current Assignee Address: JP Tokyo
- Agency: Wenderoth, Lind & Ponack, L.L.P.
- Priority: JP2011-232703 20111024
- International Application: PCT/JP2012/076786 WO 20121017
- International Announcement: WO2013/061834 WO 20130502
- Main IPC: C08G18/42
- IPC: C08G18/42 ; C08G18/00 ; C08G18/73 ; C08G63/685 ; C08G63/91 ; C08G101/00

Abstract:
The present invention relates to a method for producing an aliphatic polyester having an increased molecular weight comprising the steps of: (i) introducing into a mixing tank equipped with an inlet for injecting a diisocyanate an aliphatic polyester prepolymer which has a number average molecular weight of 5000 or higher and has terminal hydroxyl groups and in which at least one acid component is a succinic acid compound, wherein the aliphatic polyester prepolymer is introduced above the position of the inlet and wherein the aliphatic polyester prepolymer is melted at a temperature not lower than a melting point of the prepolymer and is in a liquid state, (ii) injecting a diisocyanate into the aliphatic polyester prepolymer, wherein the amount of diisocyanate is equivalent to between one tenth and two times the amount of the hydroxyl groups in the aliphatic polyester prepolymer; and (iii) reacting the aliphatic polyester prepolymer with the diisocyanate.
Public/Granted literature
- US20140275437A1 METHOD FOR PRODUCING AN ALIPHATIC POLYESTER HAVING INCREASED MOLECULAR WEIGHT Public/Granted day:2014-09-18
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