Invention Grant
- Patent Title: Method for producing surface-modified rare earth metal-based sintered magnet and surface-modified rare earth metal-based sintered magnet
- Patent Title (中): 表面改性稀土金属类烧结磁体和表面改性稀土金属类烧结磁体的制造方法
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Application No.: US12680312Application Date: 2008-09-26
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Publication No.: US09175376B2Publication Date: 2015-11-03
- Inventor: Mahoro Fujihara , Koshi Yoshimura , Atsushi Kikugawa
- Applicant: Mahoro Fujihara , Koshi Yoshimura , Atsushi Kikugawa
- Applicant Address: JP Tokyo
- Assignee: HITACHI METALS, LTD.
- Current Assignee: HITACHI METALS, LTD.
- Current Assignee Address: JP Tokyo
- Agency: Kratz, Quintos & Hanson, LLP
- Priority: JP2007-252624 20070927; JP2008-091830 20080331
- International Application: PCT/JP2008/067527 WO 20080926
- International Announcement: WO2009/041639 WO 20090402
- Main IPC: H01F1/055
- IPC: H01F1/055 ; C23C8/16 ; C23C8/12 ; H01F41/02 ; H01F1/057

Abstract:
An objective of the present invention is to provide a rare earth metal-based sintered magnet having imparted thereto sufficient corrosion resistance by an oxidative heat treatment, which is resistant even in an environment of fluctuating humidity, while suppressing the deterioration of the magnetic characteristics ascribed to the oxidative heat treatment, and to provide a method for producing the same. As a means of achieving the objective above, the surface-modified rare earth metal-based sintered magnet of the present invention is characterized in that the surface-modified part comprises a surface-modified layer comprising at least three layers formed in this order from the inner side of the magnet, a main layer containing R, Fe, B, and oxygen, an amorphous layer containing at least R, Fe, and oxygen, and an outermost layer containing iron oxide comprising mainly hematite as the constituent, and the method for producing the same is characterized in that it comprises a step of applying a heat treatment to a bulk magnet body in the temperature range of from 200° C. to 600° C., under an atmosphere with oxygen partial pressure in a range of from 1×102 Pa to 1×105 Pa and water vapor partial pressure in a range of from 0.1 Pa to 1000 Pa (exclusive of 1000 Pa).
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