Invention Grant
- Patent Title: Method for the production of D,L-methionine
- Patent Title (中): 生产D,L-甲硫氨酸的方法
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Application No.: US14671435Application Date: 2015-03-27
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Publication No.: US09206121B2Publication Date: 2015-12-08
- Inventor: Dieter Buss , Martin Steurenthaler , Michael R. Rinner , Stephan Kretz , Hans Joachim Hasselbach , Caspar-Heinrich Finkeldei , Martin Koerfer , Pablo Zacchi
- Applicant: Dieter Buss , Martin Steurenthaler , Michael R. Rinner , Stephan Kretz , Hans Joachim Hasselbach , Caspar-Heinrich Finkeldei , Martin Koerfer , Pablo Zacchi
- Applicant Address: DE Essen
- Assignee: EVONIK DEGUSSA GmbH
- Current Assignee: EVONIK DEGUSSA GmbH
- Current Assignee Address: DE Essen
- Agency: Oblon, McClelland, Maier & Neustadt, L.L.P.
- Main IPC: C07C319/20
- IPC: C07C319/20 ; C07C51/08 ; C07C253/00

Abstract:
A method to produce D,L-Methionine from 2-hydroxy-4-(methylthio)butyronitrile by reaction with ammonia, optionally in the presence of carbon dioxide, is provided. The 2-hydroxy-4-(methylthio)butyronitrile is obtained by reaction of 3-methylmercaptopropionaldehyde with hydrogen cyanide in the presence of a base as catalyst in a main reaction zone of a multizone reactor. Residual gaseous hydrogen cyanide is removed from the main reaction zone to an absorption and post-reaction zone of the reactor which comprises a mixture of 3-methylmercaptopropionaldehyde and the catalyst; and the gaseous hydrogen cyanide is further reacted with the 3-methylmercaptopropionaldehyde in the absorption and post reaction zone. A molar ratio of hydrogen cyanide to 3-(methylthio)propanal in the main reaction zone is from 0.98 to 1.03.
Public/Granted literature
- US20150197489A1 METHOD FOR THE PRODUCTION OF D,L-METHIONINE Public/Granted day:2015-07-16
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