Invention Grant
- Patent Title: Cyclic process for wet-chemically producing lithium metal phosphates
- Patent Title (中): 湿化学生产锂金属磷酸盐的循环方法
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Application No.: US11908832Application Date: 2006-03-17
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Publication No.: US09242864B2Publication Date: 2016-01-26
- Inventor: Gerhard Nuspl , Christian Vogler , Josefine Zuber
- Applicant: Gerhard Nuspl , Christian Vogler , Josefine Zuber
- Applicant Address: GB London
- Assignee: JOHNSON MATTHEY PLC
- Current Assignee: JOHNSON MATTHEY PLC
- Current Assignee Address: GB London
- Agency: Millen, White, Zelano & Branigan, P.C.
- Priority: DE102005012640 20050318
- International Application: PCT/EP2006/002472 WO 20060317
- International Announcement: WO2006/097324 WO 20060921
- Main IPC: C01B25/30
- IPC: C01B25/30 ; C01B25/45 ; C01B25/37

Abstract:
The invention relates to a method for producing lithium metal phosphates of a formula LiMPO4, wherein M is at least one type of bivalent metal, preferably selected from the first transition metal range. The inventive method consists in reacting a lithium phosphate with a metal salt and an acid phosphate source in a polar solvent for converting into a corresponding M-containing phosphate, in adding a basic lithium source for obtaining a precursor mixture for a desired lithium metal phosphate, in converting and separating the thus obtained mixture, preferably in hydrothermal conditions, in such a way that a desired final product is obtained, thereby receiving a lithium-containing filtrate. The addition of the basic lithium source initiates a lithium ion precipitation in the form of a lithium phosphate. The thus obtainable lithium phosphate can be reused in the form of a raw material, whereby said cycle enables lithium to be highly reusable.
Public/Granted literature
- US20090117022A1 CYCLIC PROCESS FOR WET-CHEMICALLY PRODUCING LITHIUM METAL PHOSPHATES Public/Granted day:2009-05-07
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