Invention Grant
- Patent Title: Method for preparing 2,3,3,3-tetrafluoropropene
- Patent Title (中): 制备2,3,3,3-四氟丙烯的方法
-
Application No.: US14967242Application Date: 2015-12-11
-
Publication No.: US09346724B2Publication Date: 2016-05-24
- Inventor: Jun Lei , Bo Yang , Yan Zhang , Yang Zhao , Huadong Zhou , Qiang Zhou , Gang Su
- Applicant: Zhejiang Quhua Fluor-Chemistry Co., Ltd.
- Applicant Address: CN Quzhou
- Assignee: Zhejiang Quhua Fluor-Chemistry Co., Ltd.
- Current Assignee: Zhejiang Quhua Fluor-Chemistry Co., Ltd.
- Current Assignee Address: CN Quzhou
- Agency: Matthias Scholl, PC
- Agent Matthias Scholl
- Priority: CN201410388875 20140808
- Main IPC: C07C17/20
- IPC: C07C17/20 ; C07C17/00 ; C07C17/383 ; C07C21/18 ; C07C17/087

Abstract:
A method for preparing 2,3,3,3-tetrafluoropropene, including: a) heating and vaporizing hydrogen fluoride and 1,1,2,3-tetrachloropropene (TCP), and introducing hydrogen fluoride and TCP to a first reactor for reaction in the presence of an A-type catalyst to yield a first product mixture including 2,3-dichloro-3,3-difluoropropene (“HCFO-1232xf”), where the mole ratio between hydrogen fluoride and TCP is between 5:1 and 60:1, the reaction temperature is between 200 and 500° C., and the space velocity is between 200 and 2000 h−1; b) preheating the first product mixture including HCFO-1232xf, introducing the first product mixture including HCFO-1232xf to a second reactor for reaction in the presence of a B-type catalyst to yield a second product mixture including HFO-1234yf, where the temperature of the preheated first product mixture including HCFO-1232xf is higher than the reaction temperature of the first reactor and lower than the reaction temperature of the second reactor.
Public/Granted literature
- US20160096787A1 METHOD FOR PREPARING 2,3,3,3-TETRAFLUOROPROPENE Public/Granted day:2016-04-07
Information query