Invention Grant
- Patent Title: Process for flashing a reaction medium
- Patent Title (中): 闪烁反应介质的方法
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Application No.: US14874268Application Date: 2015-10-02
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Publication No.: US09382183B1Publication Date: 2016-07-05
- Inventor: Ronald D. Shaver , Yaw-Hwa Liu , Mark O. Scates
- Applicant: Celanese International Corporation
- Applicant Address: US TX Irving
- Assignee: CELANESE INTERNATIONAL CORPORATION
- Current Assignee: CELANESE INTERNATIONAL CORPORATION
- Current Assignee Address: US TX Irving
- Agency: Kilpatrick Townsend & Stockton LLP
- Main IPC: C07C51/12
- IPC: C07C51/12 ; C07C51/44

Abstract:
A process for producing acetic acid is disclosed in which the methyl iodide concentration is maintained in the vapor product stream formed in a flashing step. The methyl iodide concentration in the vapor product stream ranges from 24 to less than 36 wt. %, based on the weight of the vapor product stream. In addition, the acetaldehyde concentration is maintained within the range from 0.005 to 1 wt. % in the vapor product stream. The vapor product stream is distilled in a first column to obtain an acetic acid product stream comprising acetic acid and hydrogen iodide in an amount of less than or equal to 300 wppm and/or methyl iodide in an amount from 0.1 to 6 wt. %, and an overhead stream comprising methyl iodide, water and methyl acetate.
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