Invention Grant
- Patent Title: Method for measuring the thermal stability of a succinic acid crystal intended for the production of polymers
- Patent Title (中): 用于测量用于生产聚合物的琥珀酸晶体的热稳定性的方法
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Application No.: US14381326Application Date: 2013-03-01
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Publication No.: US09534078B2Publication Date: 2017-01-03
- Inventor: Guillaume Fiey , Marilyne Guillemant , Jean-Michel Roturier , Nicolas Jacquel
- Applicant: Guillaume Fiey , Marilyne Guillemant , Jean-Michel Roturier , Nicolas Jacquel
- Applicant Address: FR Lestrem
- Assignee: ROQUETTE FRERES
- Current Assignee: ROQUETTE FRERES
- Current Assignee Address: FR Lestrem
- Agency: Young & Thompson
- Priority: FR1251924 20120302
- International Application: PCT/FR2013/050438 WO 20130301
- International Announcement: WO2013/144471 WO 20131003
- Main IPC: G01N21/25
- IPC: G01N21/25 ; C08G63/16 ; G01N21/84 ; C07C51/50 ; C08G63/78 ; G01N21/29 ; G01N21/94

Abstract:
A method for measuring the thermal stability of succinic acid includes the following steps: 1) preparing a succinic acid crystal powder having less than 1% residual water content; 2) placing 10 g of the crystal powder in an oven at 220° C. for 2 hours; 3) pulverizing and sieving the crystal powder processed in this way, such that the particle size distribution thereof is between 0 and 10%, and preferably between 4 and 6% for particles larger than 500 μm in size, between 20 and 40%, and preferably between 25 and 35% for particles between 200 and 500 μm in size, between 50 and 75% and preferably between 55 and 70% for particles smaller than 200 μm in size; and 4) measuring the color, in a spectrocolorimeter, of the pulverized and sieved powder and determining the average value of the yellow (index “b”).
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