A calibration source for a gamma-ray spectrometer is provided, comprising a scintillator body having a cavity in which a radioactive material is received. A scintillator body may be cuboid and the cavity may be a hole drilled into the scintillator body. The radioactive material comprises an isotope having a decay transition associated with emission of a radiation particle and a gamma-ray of known energy. A photodetector is optically coupled to the scintillator body and arranged to detect scintillation photons generated when radiation particles emitted from the radioactive material interact with the surrounding scintillator. A gating circuit is arranged to receive detection signals to generate corresponding gating signals for a data acquisition circuit of an associated gamma-ray spectrometer to indicate that gamma-ray detections in the gamma-ray spectrometer occurring within a time window defined by the gating signal are associated with a decay transition in the radioactive isotope.