Invention Grant
- Patent Title: Methods for synthesizing microporous crystals and microporous crystal membranes
- Patent Title (中): 合成微孔晶体和微孔结晶膜的方法
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Application No.: US14194199Application Date: 2014-02-28
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Publication No.: US09561477B2Publication Date: 2017-02-07
- Inventor: Prabir Dutta , Michael Severance , Chenhu Sun
- Applicant: OHIO STATE INNOVATION FOUNDATION
- Applicant Address: US OH Columbus
- Assignee: Ohio State Innovation Foundation
- Current Assignee: Ohio State Innovation Foundation
- Current Assignee Address: US OH Columbus
- Agency: Meunier Carlin & Curfman LLC
- Main IPC: C01B39/54
- IPC: C01B39/54 ; C01B39/02 ; B01D71/02 ; C01B39/22 ; C01B39/38 ; B01J29/40 ; B01J37/02 ; B01J29/08 ; C01B39/20 ; C01B39/24 ; C01B39/40 ; B01D67/00

Abstract:
A method of making a microporous crystal material, comprising: a. forming a mixture comprising NaOH, water, and one or more of an aluminum source, a silicon source, and a phosphate source, whereupon the mixture forms a gel; b. heating the gel for a first time period, whereupon a first volume of water is removed from the gel and micoroporous crystal nuclei form, the nuclei having a framework; and c.(if a membrane is to be formed) applying the gel to a solid support seeded with microporous crystals having a framework that is the same as the framework of the nuclei; d. heating the gel for a second time period. during which a second volume of water is added to the gel; wherein the rate of addition of the second volume of water is between about 0.5 and about 2.0 fold the rate of removal of the first volume of water.
Public/Granted literature
- US20140241981A1 METHODS FOR SYNTHESIZING MICROPOROUS CRYSTALS AND MICROPOROUS CRYSTAL MEMBRANES Public/Granted day:2014-08-28
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