Invention Grant
US09562027B2 Device and method for continuously preparing high-purity AKD without solvent
有权
无溶剂连续制备高纯度AKD的装置和方法
- Patent Title: Device and method for continuously preparing high-purity AKD without solvent
- Patent Title (中): 无溶剂连续制备高纯度AKD的装置和方法
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Application No.: US14649703Application Date: 2013-03-12
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Publication No.: US09562027B2Publication Date: 2017-02-07
- Inventor: Baochi Sun , Anqi Tan
- Applicant: SUZHOU TIANMA SPECIALTY CHEMICALS CO., LTD.
- Applicant Address: CN Jiangsu
- Assignee: SUZHOU TIANMA SPECIALTY CHEMICALS CO., LTD.
- Current Assignee: SUZHOU TIANMA SPECIALTY CHEMICALS CO., LTD.
- Current Assignee Address: CN Jiangsu
- Agency: Oliff PLC
- Priority: CN201210513320 20121204
- International Application: PCT/CN2013/072498 WO 20130312
- International Announcement: WO2014/086122 WO 20140612
- Main IPC: C07D305/08
- IPC: C07D305/08 ; B01J19/18 ; B01J19/00 ; B01J19/20 ; C07D305/12 ; B01F7/04 ; C07C45/89 ; C07C49/88

Abstract:
Device and method for continuously preparing high-purity AKD without solvent includes a reactor making continuous mixing of raw materials. The process includes: the tertiary amine feeding into the reactor and the continuously feeding acyl chloride from three to ten line; under operating state, the motor rotates the internal cylinder in relation to external cylinder, forcing the fed materials to convey and stir in the conveying section of annular column passage, forcing the materials to shear and mix by movement of shearing and kneading blades. Arrangement of conveying and mixing sections along the axial direction of annular column passage, causes sufficient reaction of materials and controls the material temperature through internal and external heat exchange systems until the reaction products are discharged from outlet. The device and process disperse reaction heat and sufficient material mixture and complete reaction to control the reaction temperature, viscosity and decrease the generation of side reaction.
Public/Granted literature
- US20150315163A1 DEVICE AND METHOD FOR CONTINUOUSLY PREPARING HIGH-PURITY AKD WITHOUT SOLVENT Public/Granted day:2015-11-05
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