Invention Grant
US09567434B2 Process for preparing PA-4X, and PA-410 obtainable by the process
有权
制备可通过该方法获得的PA-4X和PA-410的方法
- Patent Title: Process for preparing PA-4X, and PA-410 obtainable by the process
- Patent Title (中): 制备可通过该方法获得的PA-4X和PA-410的方法
-
Application No.: US13696336Application Date: 2011-05-05
-
Publication No.: US09567434B2Publication Date: 2017-02-14
- Inventor: Pim Gerard Anton Janssen , Ronald Ligthart
- Applicant: Pim Gerard Anton Janssen , Ronald Ligthart
- Applicant Address: NL Heerlen
- Assignee: DSM IP ASSETS B.V.
- Current Assignee: DSM IP ASSETS B.V.
- Current Assignee Address: NL Heerlen
- Agency: Nixon & Vanderhye P.C.
- Priority: EP10162132 20100506
- International Application: PCT/EP2011/057208 WO 20110505
- International Announcement: WO2011/138397 WO 20111110
- Main IPC: C08G69/26
- IPC: C08G69/26 ; C08G69/00 ; C08L77/06 ; C08G69/46 ; C08G69/28

Abstract:
A process for preparation of a polyamide PA-4X containing monomer units of 1,4-diaminobutane and an aliphatic linear dicarboxylic acid X with at least 8 carbon atoms, which contains the following steps: 1) making a solution comprising a salt of 1,4-diaminobutane and the aliphatic linear dicarboxylic acid and water, at a temperature at which the salt dissolves; 2) concentrating the solution of the salt at a temperature above the crystallization temperature of the salt, at a pressure of at most 7 barA to a water content of between 0 and 30 wt % based on the total amount of solution, 3) producing a polymer from the solution obtained by step 2, while keeping the polymer in a melt and at a pressure of less than 18 barA, 4) depressurizing the polymer obtained at step 3 while keeping the polymer in the melt to further polymerize the polymer. In an preferred embodiment the aliphatic linear dicarboxylic acid is 1,10-decanedioic acid. Also claimed is a polyamide 410 having a viscosity number (VN) of at least 100 ml/gram.
Public/Granted literature
- US20130131307A1 PROCESS FOR PREPARING PA-4X, AND PA-410 OBTAINABLE BY THE PROCESS Public/Granted day:2013-05-23
Information query