Invention Grant
US09586894B2 Preparation method of solid acrylamidealkyl sulfonate 有权
固体丙烯酰胺烷基磺酸盐的制备方法

  • Patent Title: Preparation method of solid acrylamidealkyl sulfonate
  • Patent Title (中): 固体丙烯酰胺烷基磺酸盐的制备方法
  • Application No.: US14765315
    Application Date: 2014-01-24
  • Publication No.: US09586894B2
    Publication Date: 2017-03-07
  • Inventor: Longyuan Mei
  • Applicant: Longyi Mei
  • Applicant Address: CN Nanjing
  • Assignee: Longyi Mei
  • Current Assignee: Longyi Mei
  • Current Assignee Address: CN Nanjing
  • Agency: Kilpatrick Townsend & Stockton LLP
  • Priority: CN201310044319 20130204
  • International Application: PCT/CN2014/071389 WO 20140124
  • International Announcement: WO2014/117685 WO 20140807
  • Main IPC: C07C303/32
  • IPC: C07C303/32 C07C303/44
Preparation method of solid acrylamidealkyl sulfonate
Abstract:
The present invention provides a method for preparing a solid acrylamide alkyl sulfonate. Said method comprises: reacting 2-acrylamido-2-methylpropanesulfonic acid and analogs thereof with an alkaline substance in a solvent. The 2-acrylamido-2-methylpropanesulfonic acid and the analogs thereof and the alkaline substance are significant excess with respect to the solvent, so that the amount of the resulting acrylamido alkyl sulfonate exceeds the solubility under the reaction condition. The acrylamido alkyl sulfonate can be continuously generated and directly massively precipitated, and the precipitated solid product, i.e. the product, is collected. The method of the present invention can greatly improve production efficiency of products, save time, reduce cost, and easy to operate by leaving out the re-crystallization step and the like in the prior art.
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