Invention Grant
- Patent Title: Process for preparing TDI isocyanurate
- Patent Title (中): 制备TDI异氰脲酸酯的方法
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Application No.: US14652242Application Date: 2014-02-11
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Publication No.: US09593089B2Publication Date: 2017-03-14
- Inventor: Xiao Zhang , Yulin Zhu , Zhenguang Wen , Kai Wang
- Applicant: Wanhua Chemical (Beijing) Co., Ltd. , Wanhua Chemical Group Co., Ltd. , Wanhua Chemical (Ningbo) Co., Ltd.
- Applicant Address: CN CN CN
- Assignee: Wanhua Chemical (Beijing) Co., Ltd.,Wanhua Chemical Group Co., Ltd.,Wanhua Chemical (Ningbo) Co., Ltd.
- Current Assignee: Wanhua Chemical (Beijing) Co., Ltd.,Wanhua Chemical Group Co., Ltd.,Wanhua Chemical (Ningbo) Co., Ltd.
- Current Assignee Address: CN CN CN
- Agency: Kramer Levin Naftalis & Frankel LLP
- Priority: CN201310099777 20130319
- International Application: PCT/CN2014/071951 WO 20140211
- International Announcement: WO2014/146522 WO 20140925
- Main IPC: C07D251/32
- IPC: C07D251/32 ; C07D251/34 ; C08G18/79 ; C08G18/02 ; C08G18/09

Abstract:
The present invention relates to a method for preparing TDI (toluene diisocyanate) isocyanurate by using TDI, monohydric alcohol, solvent, antioxidant, catalyst and termination agent as the raw materials. The properties of the isocyanurate are improved by the process comprising the modification by monohydric alcohol and addition of the catalyst and solvent in several stages at an appropriate temperature. By adding the catalyst and solvent in batches at the condition of controlling both NCO % and the viscosity in the preparation process, and adjusting the solid content at each step, the resulting TDI isocyanurate has low content of free TDI, high xylene tolerance, small product color number, and high performance stability, which makes the product obtained by the isocyanurate have good application properties such as the drying, polishing and extinction properties of coating film, and such isocyanurate has good compatibility with other components.
Public/Granted literature
- US20160016917A1 PROCESS FOR PREPARING TDI ISOCYANURATE Public/Granted day:2016-01-21
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