Invention Grant
- Patent Title: Method for producing glycolide
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Application No.: US14770900Application Date: 2014-03-18
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Publication No.: US09643949B2Publication Date: 2017-05-09
- Inventor: Kazuyuki Yamane , Yoshiko Ikeyama
- Applicant: Kureha Corporation
- Applicant Address: JP Tokyo
- Assignee: KUREHA CORPORATION
- Current Assignee: KUREHA CORPORATION
- Current Assignee Address: JP Tokyo
- Agency: Birch, Stewart, Kolasch & Birch, LLP
- Priority: JP2013-066000 20130327
- International Application: PCT/JP2014/057257 WO 20140318
- International Announcement: WO2014/156809 WO 20141002
- Main IPC: C07D319/12
- IPC: C07D319/12

Abstract:
A method for producing a GL comprising: (I) a heating step of heating a mixture either under normal pressure or reduced pressure at a temperature at which a polyglycolic acid (PGA) undergoes depolymerization, the mixture containing the PGA and a polyethylene glycol ether which is represented by the formula: X—O—(—CH2CH2—O—)p—Y (wherein X and Y are each independently an alkyl group or an aryl group having from 2 to 20 carbon atoms, and p is an integer from 1 to 5) and which has a molecular weight of from 150 to 450 and a boiling point of from 130 to 220° C. at a pressure of 3 kPa; (II) a solution-forming step in which the mixture is rendered in a solution state in which a melt phase of the PGA and a liquid phase consisting of the polyethylene glycol ether essentially form a uniform phase; (III) a GL production step in which a glycolide (GL) is produced by a depolymerization reaction of the PGA by continuing to heat the mixture in the solution state; (IV) a distillation step of distilling off the produced GL together with the polyethylene glycol ether (B) from the depolymerization reaction system; and (V) a recovery step of recovering the GL from the distillate.
Public/Granted literature
- US20160002197A1 METHOD FOR PRODUCING GLYCOLIDE Public/Granted day:2016-01-07
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