Invention Grant
- Patent Title: Division of a polyarylene ether solution
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Application No.: US14904614Application Date: 2014-07-16
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Publication No.: US09809686B2Publication Date: 2017-11-07
- Inventor: Joerg Erbes , Stefan Muessig , Tobias Kortekamp , Marco Krueger , Markus Steffen , Angela Ulzhoefer , Cecile Schneider , Alexandra Wiedemann , Simon Gramlich
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Oblon, McClelland, Maier & Neustadt, L.L.P.
- Priority: EP13176993 20130718
- International Application: PCT/EP2014/065240 WO 20140716
- International Announcement: WO2015/007774 WO 20150122
- Main IPC: C08G75/00
- IPC: C08G75/00 ; C08J3/14 ; C08J3/12 ; C08G65/46 ; C08G75/23 ; B29C47/00 ; B29K81/00

Abstract:
The invention relates to a process for producing polyarylene ether beads from a polyarylene ether solution, comprising the steps of i) dividing the polyarylene ether solution in a division apparatus which is made to vibrate with a frequency of 10 to 1400 Hz to obtain droplets, ii) transferring the droplets into a precipitation bath to form polyarylene ether beads in the precipitation bath which (A) comprises at least one aprotic solvent (component (1)) and at least one protic solvent (component (2)), (B) has a temperature of 0° C. to Tc, where the critical temperature Tc in [° C.] can be determined by the numerical equation Tc=(77−c)/0.58 in which c is the concentration of component (1) in the precipitation bath in [% by weight] and (C) has component (1) in concentrations of 5% by weight to cc, where the critical concentration cc in [% by weight] can be determined by the numerical equation cc=77−0.58*T in which T is the temperature in the precipitation bath in [° C.], where the percentages by weight are each based on the sum of the percentages by weight of component (1) and of component (2) in the precipitation bath.
Public/Granted literature
- US20160159990A1 DIVISION OF A POLYARYLENE ETHER SOLUTION Public/Granted day:2016-06-09
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