Invention Grant
- Patent Title: Process for workup of a crude ester comprising esterification catalyst hydrolysis product in suspended particulate form
-
Application No.: US15500197Application Date: 2015-07-29
-
Publication No.: US09932292B2Publication Date: 2018-04-03
- Inventor: Piotr Makarczyk , Boris Breitscheidel , Beatrice Rössler-Feigel , Kerstin Mühlheims
- Applicant: BASF SE
- Applicant Address: DE
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE
- Agency: Drinker Biddle & Reath LLP
- Priority: EP14179461 20140801
- International Application: PCT/EP2015/067337 WO 20150729
- International Announcement: WO2016/016285 WO 20160204
- Main IPC: C07C67/48
- IPC: C07C67/48 ; C07C67/56

Abstract:
In a process for workup of a crude ester comprising esterification catalyst hydrolysis product in suspended particulate form, a) the crude ester is admixed in an emulsifying tank with 1% to 10% by weight of water and the water is emulsified in the crude ester to obtain a suspoemulsion, b) the suspoemulsion from the emulsifying tank is transferred to an agglomerating tank containing an initial charge of water-undersaturated crude ester, such that a water content below the solubility limit of water in the crude ester is established in the mixture of the suspoemulsion and the initial charge of crude ester, as a result of which the suspended particulate esterification catalyst hydrolysis products form stable agglomerates, and c) the agglomerates formed are filtered off.
Public/Granted literature
Information query