Invention Grant
- Patent Title: Production method of zeolite film in which one axis is completely vertically oriented, using steam under synthetic gel-free condition
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Application No.: US14369973Application Date: 2012-12-28
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Publication No.: US09938637B2Publication Date: 2018-04-10
- Inventor: Kyung Byung Yoon , Cao Thanh Tung Pham
- Applicant: Industry-University Cooperation Foundation Sogang University
- Applicant Address: KR Seoul
- Assignee: Industry-University Cooperation Foundation Sogang University
- Current Assignee: Industry-University Cooperation Foundation Sogang University
- Current Assignee Address: KR Seoul
- Agency: Hovey Williams LLP
- Priority: KR10-2011-0147688 20111230
- International Application: PCT/KR2012/011807 WO 20121228
- International Announcement: WO2013/100734 WO 20130704
- Main IPC: C30B19/12
- IPC: C30B19/12 ; C01B39/02 ; C01B39/38 ; C30B29/34

Abstract:
Provided are a method for preparing a thin film or a thick film, including: a first step of providing a porous substrate capable of supplying silicon; a second step of applying zeolite seed crystals onto the surface of the porous substrate; a third step of coating the seed crystals-applied porous substrate with an aqueous solution containing a structure-directing agent; and a fourth step of forming and growing a film from the seed crystals by the secondary growth above a temperature at which moisture inside the seed crystals-applied porous substrate prepared in the third step can form steam, and a film prepared by the method. The film manufacturing method of the present invention is a simple manufacturing process, and thus has high reproducibility and high throughput. Since a synthetic gel is not used and a solution is used, the unnecessary consumption of materials, environmental pollution, and waste of a synthetic gel can be prevented while not necessitating drying and washing of a film.
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