HONEYCOMB BODY REACTOR PLUGGING PROCESS IMPROVEMENTS
    2.
    发明公开
    HONEYCOMB BODY REACTOR PLUGGING PROCESS IMPROVEMENTS 审中-公开
    改进密封程序蜂窝体反应器

    公开(公告)号:EP2539302A1

    公开(公告)日:2013-01-02

    申请号:EP11707534.1

    申请日:2011-02-28

    Abstract: A method is disclosed for plugging selected cells of a honeycomb monolith so as to form a fluidic reactor, the method comprising contacting selected cells of a honeycomb monolith with a melted or softened plug material, the material comprising at least one sinterable particulate and a binder, the binder comprising at least one thermo-setting component and at least one UV-radiation curable polymer, the contacting performed such that a portion of the material remains in contact with the selected cells and plugs the selected cells; cooling the melted or softened plug material such that the thermo-setting component sets; after cooling, irradiating the portion of the material so as to at least partially cure the radiation curable polymer; and after irradiating, debinding or debinding and sintering the portion of the material so as to remove the binder or s as to debind and sinter the at least one sinterable particulate, wherein the step of debinding or debinding and sintereing is performed with the cells of the monolith in a vertical orientation resting on a flat surface with a compatible ceramic or other refractory material felt covering the openings below and above and with a weight resting on the upper face, with optional shims defining the distance between the felt and the end faces.

    HONEYCOMB BODY REACTOR PLUGGING PROCESS IMPROVEMENTS
    7.
    发明申请
    HONEYCOMB BODY REACTOR PLUGGING PROCESS IMPROVEMENTS 审中-公开
    蜂窝体反应器插入过程改进

    公开(公告)号:WO2011106758A1

    公开(公告)日:2011-09-01

    申请号:PCT/US2011/026397

    申请日:2011-02-28

    Abstract: A method is disclosed for plugging selected cells of a honeycomb monolith so as to form a fluidic reactor, the method comprising contacting selected cells of a honeycomb monolith with a melted or softened plug material, the material comprising at least one sinterable particulate and a binder, the binder comprising at least one thermo-setting component and at least one UV-radiation curable polymer, the contacting performed such that a portion of the material remains in contact with the selected cells and plugs the selected cells; cooling the melted or softened plug material such that the thermo-setting component sets; after cooling, irradiating the portion of the material so as to at least partially cure the radiation curable polymer; and after irradiating, debinding or debinding and sintering the portion of the material so as to remove the binder or s as to debind and sinter the at least one sinterable particulate, wherein the step of debinding or debinding and sintereing is performed with the cells of the monolith in a vertical orientation resting on a flat surface with a compatible ceramic or other refractory material felt covering the openings below and above and with a weight resting on the upper face, with optional shims defining the distance between the felt and the end faces.

    Abstract translation: 公开了一种用于堵塞蜂窝状整料的所选择的细胞以形成流体反应器的方法,该方法包括将蜂窝状整料的选定的细胞与熔融或软化的塞子材料接触,所述材料包括至少一种可烧结颗粒和粘合剂, 所述粘合剂包含至少一种热固性组分和至少一种UV辐射固化聚合物,所述接触进行使得所述材料的一部分保持与所选择的电池接触并堵塞所选择的电池; 冷却熔融或软化的塞子材料,使得热固性成分组合; 在冷却之后,照射材料的该部分以至少部分地固化可辐射固化的聚合物; 并且在照射,脱脂或脱脂并烧结该材料的该部分之后,以除去粘合剂,以便剥离和烧结该至少一个可烧结颗粒,其中脱粘或脱脂和引发步骤是用 整块材料在垂直方向上放置在平坦表面上,其中相容的陶瓷或其它难熔材料毡覆盖下方和上方的开口,并且具有搁置在上表面上的重物,并且可选的垫片限定了毡和端面之间的距离。

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