Abstract:
본 발명은 전극재료 합성방법에 관한 것으로, 보다 구체적으로는 초급속연소법을 이용함으로써 전극재료를 합성하는 데 필요한 반응결과물의 열처리 공정 및 기타 부가과정인 세정, 필터링 및 건조 단계가 전혀 필요하지 않아 결과물을 얻는데 수초 내지 수분밖엔 소요되지 않는 초급속연소법를 이용한 나노전극재료 합성방법 및 그 방법으로 합성된 나노전극재료에 관한 것이다.
Abstract:
PURPOSE: A synthesis method of a nanoelectrode material, and the nanoelectrode material synthesized therefrom are provided to secure the excellent crystalline property of the material only by synthesizing at room temperature. CONSTITUTION: A synthesis method of a nanoelectrode material comprises the following steps: mixing a polyol solvent, a transition metal oxide, a polyacid anion-based compound, a lithium system compound, and a flammable liquid, to form a reaction solution; combusting the reaction solution; and collecting particles after combusting to obtain the nanoelectrode material.
Abstract:
A cathode material of a lithium secondary battery and a manufacturing method thereof are provided to realize high-capacity while suppressing transition to a spinel phase during several times cycle process through the partial substitution of transition metal having low valent metal in a LiM'M"O3 structure, or model metal. A method for manufacturing a cathode material of a lithium secondary battery comprises (S110) a step for obtaining a lithium precursor, M' precursor and M'' precursor by dissolving the lithium precursor, M' precursor and M'' precursor in distilled water respectively; (S120) a step for obtaining the M'M'' precursor solution by adding M'' precursor solution in M' precursor; (S130) a step for obtaining the lithium M'M'' precursor solution by adding the lithium precursor solution in the M'M'' precursor solution; (S140) a step for agitating the lithium M'M'' precursor solution; (S150) a step for obtaining parent powder by putting the agitated lithium M'M'' precursor solution in an oven, and evaporating water from the M'M'' precursor solution; (S160) a step for pulverizing the parent powder and to heating it to the first temperature in the atmosphere; (S170) a step for heating the parent powder at the second temperature higher than the first temperature and cooling it; and (S180) a step for obtaining a cathode material of a lithium secondary battery by washing the cooled parent powder with distilled water and drying the washed parent powder.
Abstract:
A cathode material of a lithium-ion battery and a manufacturing method thereof is provided to realize high-capacity while suppressing transition to a spinel phase by bonding oxygen through the partial substitution of transition metal having low valent metal in a LiM'M''O3 structure, or model metal. A method for manufacturing a cathode material of a lithium secondary battery comprises (S110) a step for manufacturing a lithium precursor, M' precursor and M'' precursor by dissolving the lithium precursor, M' precursor and M'' precursor in distilled water respectively; (S120) a step for manufacturing the M'M'' precursor solution by adding M'' precursor solution in M' precursor; (S130) a step for manufacturing the lithium M'M'' precursor solution by adding the lithium precursor solution in the M'M'' precursor solution; (S140) a step for agitating the lithium M'M'' precursor solution; (S150) a step for obtaining parent powder by putting the agitated lithium M'M'' precursor solution in an oven, and evaporating water from the M'M'' precursor solution; (S160) a step for pulverizing the parent powder and to heating it to the first temperature in the atmosphere; (S170) a step for heating the parent powder at the second temperature higher than the first temperature and cooling it; and (S180) a step for obtaining a cathode material of a lithium secondary battery by washing the cooled parent powder with distilled water and drying the washed parent powder.