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1.发明申请
公开(公告)号：WO2023079414A1
公开(公告)日：2023-05-11
申请号：PCT/IB2022/060291
申请日：2022-10-26
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HIRSCHBERG, Markus E. , MUGGLI, Mark W. , PAJKERT, Romana M. , RÖSCHENTHALER, Gerd-Voker , TVERDOMED, Sergey N.
Abstract: Described herein is method of making a multifunctional compound by starting with a H-(OR)n-P(=O)(ORh1)2 and performed a series of reactions to form a functionalized phosphorous compound such as CF2=CF-CFY2-(OR)n-P(=O)(OQ)2 (VIIA) CF2X3CF=CF-(OR)n-P(=O)(OQ)2 (VIIB), or CF2X3CHFC(=O)-(OR)n-P(=O)(OH)2 (VIB) Where: R is a C1-C4 alkenyl group; X3 is F or -(OR)n-P(=O)(OQ)2; n is 0 or 1; Y2 is -F, -Cl, -Br, -H, or a fluoroalkyl group comprising 1 to 3 carbon atoms, wherein the fluoroalkyl group optionally comprises at least one of an ether linkage, Cl, Br, or I; and Q is an alkyl group having 1 to 6 carbon atoms and optionally comprising at least one catenated ether linkage, -Si(CH3)3, -Si(CH2CH3)3, -H, a metallic cation, or a quaternary ammonium cation can be disposed on a metal surface. Such compounds may be used in generating ionomeric polymers and/or applied onto metal substrates.
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公开(公告)号：WO2018211457A3
公开(公告)日：2018-11-22
申请号：PCT/IB2018/053488
申请日：2018-05-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HINTZER, Klaus , HIRSCHBERG, Markus E. , PAJKERT, Romana , RÖSCHENTHALER, Gerd-Volker , TVERDOMED, Sergey N.
IPC: C07C41/14 , C07C303/26 , C07C309/06 , C07C43/12
Abstract: A method includes combining first components including at least one of CF 2 =CF-CF 2 -OSO 2 Cl or CF 2 =CF-CF 2 -OSO 2 CF 3 , a polyfluorinated compound having at least one ketone or carboxylic acid halide, and fluoride ion to provide a compound comprising at least one perfluorinated allyl ether group. A method includes combining second components including B(OSO 2 Cl) 3 and hexafluoropropylene to provide CF 2 =CF-CF 2 -OSO 2 Cl. Another method includes combining second components including M(OSO 2 CF 3 ) 3 and hexafluoropropylene at a temperature above 0 ˚C to provide CF 2 =CF-CF 2 -OSO 2 CF 3 , wherein M is Al or B. The compound CF 2 =CF-CF 2 -OSO 2 Cl is also provided.
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3.发明申请CONVERSION OF A PERFLUORINATED VINYL ETHER INTO A PARTIALLY FLUORINATED SATURATED ETHER DERIVATIVE 审中-公开将全氟乙烯醚转化为部分氟化的饱和醚衍生物
公开(公告)号：WO2017112629A1
公开(公告)日：2017-06-29
申请号：PCT/US2016/067674
申请日：2016-12-20
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HIRSCHBERG, Markus E. , HINTZER, Klaus , QIU, Zai-Ming , RÖSCHENTHALER, Gerd-Volker , PAJKERT, Romana , TVERDOMED, Sergey N.
IPC: C07C41/18 , C07C41/30 , C07C249/02 , C07C253/18
CPC classification number: C07C249/02 , C07C41/18 , C07C41/30 , C07C253/18 , C07C43/126 , C07C251/08 , C07C255/13
Abstract: Methods of converting a fluorinated vinyl ether to a saturated partially fluorinated ether, the method comprising: reacting the fluorinated vinyl ether with an amine, ammonia, or combination thereof to form the saturated partially fluorinated ether.
Abstract translation: 将氟化乙烯基醚转化为饱和部分氟化醚的方法，所述方法包括：使氟化乙烯基醚与胺，氨或其组合反应以形成饱和部分氟化醚。 p>
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4.发明申请
公开(公告)号：WO2020245724A1
公开(公告)日：2020-12-10
申请号：PCT/IB2020/055202
申请日：2020-06-02
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HIRSCHBERG, Markus E. , HINTZER, Klaus , RÖSCHENTHALER, Gerd-Volker , TVERDOMED, Sergey N. , PAJKERT, Romana
IPC: C07F7/18 , C07C67/00 , C08F220/24 , C08G65/00
Abstract: The multifunctional compound is represented by formula X-C(R)RF-Y, in which X and Y are each independently -C(O)-O-M, -C(O)-HAL, -C(O)-NR 1 2 , -C≡N, -C(O)NR 1 -SO 2 -R f 1 -W, or a fluorinated alkenyl group that is optionally interrupted by one or more -O- groups. HAL is -F, -Cl, or -Br. R f 1 is a fluorinated alkylene group that is optionally interrupted by one or more -O- groups. W is -F, -SO 2 Z, -CF=CF 2 , -O-CF=CF 2 , or -O-CF 2 -CF=CF 2 . Z is -F, - Cl, -NR 1 2 , or -OM. Each R 1 is a hydrogen atom or alkyl having up to four carbon atoms. M is an alkyl group, a trimethylsilyl group, a hydrogen atom, a metallic cation, or a quaternary ammonium cation. R is a bromine, chloride, fluorine or hydrogen atom; and RF is a fluorinated alkenyl group that is unsubstituted or substituted by at least one chlorine atom, aryl group, or a combination thereof or RF is a fluorinated alkyl group or arylalkylenyl group that is substituted by bromine or iodine and uninterrupted or interrupted by at least one -O- group. A process for making the compound is also disclosed. A fluoropolymer made from the compound and a method of making the fluoropolymer are also disclosed.
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公开(公告)号：WO2019123342A1
公开(公告)日：2019-06-27
申请号：PCT/IB2018/060386
申请日：2018-12-19
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HIRSCHBERG, Markus E. , HINTZER, Klaus , LAMANNA, William M. , SMITH, Sean M. , RÖSCHENTHALER, Gerd-Volker , PAJKERT, Romana , TVERDOMED, Sergey N.
IPC: C07C51/31
Abstract: A method of making a polyfunctional polyfluorinated compound includes combining first components that include a polyfluorinated cyclic compound having 4 to 7 ring carbon atoms and at least one of osmium tetroxide, ruthenium tetroxide or a precursor thereof and forming a polyfluorinated dicarboxylic acid. Two of the ring carbon atoms of the polyfluorinated cyclic compound form a double bond or an epoxide. The precursor reacts with an oxidant to form ruthenium tetroxide. Methods also include converting the polyfluorinated dicarboxylic acid to a polyfluorinated dicarboxylic acid halide and converting the polyfluorinated dicarboxylic acid halide to other polyfunctional polyfluorinated compounds.
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Patent Agency Ranking
公开(公告)号：WO2018211457A2
公开(公告)日：2018-11-22
申请号：PCT/IB2018/053488
申请日：2018-05-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY
Inventor： HINTZER, Klaus , HIRSCHBERG, Markus E. , PAJKERT, Romana , RÖSCHENTHALER, Gerd-Volker , TVERDOMED, Sergey N.
IPC: C07C41/14 , C07C303/26 , C07C309/06 , C07C43/12
Abstract: A method includes combining first components including at least one of CF 2 =CF-CF 2 -OSO 2 Cl or CF 2 =CF-CF 2 -OSO 2 CF 3 , a polyfluorinated compound having at least one ketone or carboxylic acid halide, and fluoride ion to provide a compound comprising at least one perfluorinated allyl ether group. A method includes combining second components including B(OSO 2 Cl) 3 and hexafluoropropylene to provide CF 2 =CF-CF 2 -OSO 2 Cl. Another method includes combining second components including M(OSO 2 CF 3 ) 3 and hexafluoropropylene at a temperature above 0 ˚C to provide CF 2 =CF-CF 2 -OSO 2 CF 3 , wherein M is Al or B. The compound CF 2 =CF-CF 2 -OSO 2 Cl is also provided.
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公开(公告)号：EP3625201A2
公开(公告)日：2020-03-25
申请号：EP18730859.8
申请日：2018-05-17
Applicant: 3M Innovative Properties Company
Inventor： HINTZER, Klaus , HIRSCHBERG, Markus E. , PAJKERT, Romana , R SCHENTHALER, Gerd-Volker , TVERDOMED, Sergey N.
IPC: C07C41/14 , C07C303/26 , C07C309/06 , C07C43/12
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公开(公告)号：EP3728177A1
公开(公告)日：2020-10-28
申请号：EP18840071.7
申请日：2018-12-19
Applicant: 3M Innovative Properties Company
Inventor： HIRSCHBERG, Markus E. , HINTZER, Klaus , LAMANNA, William M. , SMITH, Sean M. , RÖSCHENTHALER, Gerd-Volker , PAJKERT, Romana , TVERDOMED, Sergey N.
IPC: C07C51/31
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9.发明公开
公开(公告)号：EP3394021A1
公开(公告)日：2018-10-31
申请号：EP16831671.9
申请日：2016-12-20
Applicant: 3M Innovative Properties Company
Inventor： HIRSCHBERG, Markus E. , HINTZER, Klaus , QIU, Zai-Ming , RÖSCHENTHALER, Gerd-Volker , PAJKERT, Romana , TVERDOMED, Sergey N.
IPC: C07C41/18 , C07C41/30 , C07C249/02 , C07C253/18
CPC classification number: C07C249/02 , C07C41/18 , C07C41/30 , C07C253/18 , C07C43/126 , C07C251/08 , C07C255/13
Abstract: Methods of converting a fluorinated vinyl ether to a saturated partially fluorinated ether, the method comprising: reacting the fluorinated vinyl ether with an amine, ammonia, or combination thereof to form the saturated partially fluorinated ether.
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10.发明公开
公开(公告)号：EP4429886A1
公开(公告)日：2024-09-18
申请号：EP22801232.4
申请日：2022-10-26
Applicant: 3M Innovative Properties Company
Inventor： HIRSCHBERG, Markus E. , MUGGLI, Mark W. , PAJKERT, Romana M. , RÖSCHENTHALER, Gerd-Voker , TVERDOMED, Sergey N.
CPC classification number: C07F9/4006 , C07F9/3808 , C07F9/409 , H01M10/0565 , H01M8/1018 , H01M10/052 , H01M2300/008220130101 , C08F230/02 , C08F130/02 , C08F216/1408 , C08F216/1475 , Y02E60/50 , Y02P70/50
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