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    CROSSLINKING COMPOSITION HAVING A POLYROTAXANE AND A COMPOUND HAVING TWO OR MORE OXIRANE GROUPS AND/OR OXETANE GROUPS
    105.
    发明公开
    CROSSLINKING COMPOSITION HAVING A POLYROTAXANE AND A COMPOUND HAVING TWO OR MORE OXIRANE GROUPS AND/OR OXETANE GROUPS 审中-公开
    跟组成聚轮烷有两个或更多的环氧乙烷和/或氧杂环丁烷的连接

    公开(公告)号：EP3006480A1

    公开(公告)日：2016-04-13

    申请号：EP14808429.6

    申请日：2014-06-06

    Applicant: Advanced Softmaterials Inc.

    Inventor： HAYASHI, Yuki

    IPC: C08G59/40 ,  C08G65/18 ,  C08L63/00 ,  C08L71/02

    CPC classification number: C09J167/04 ,  C08G59/5033 ,  C09D167/04

    Abstract: The present invention provides a material of high toughness that could not have been provided by an epoxy resin alone. The present invention provides a crosslinking composition having (A) one or more polyrotaxanes in which end-capping groups which prevent dissociation of the linear group are situated at both ends of a pseudo-polyrotaxane formed by inclusion of a linear molecule in the opening of a cyclic molecule by being threaded therethrough, the polyrotaxane having on the cyclic molecule a functional group that is capable of reacting with the oxirane group and/or the oxetane group, the functional group being one or more selected from the group consisting of carboxylic acid groups, carboxylate groups, primary amine groups, secondary amino groups, tertiary amino groups, phenol groups, the oxirane group, and the oxetane group, and (B) a compound having two or more oxirane groups and/or oxetane groups; and a crosslinked product employing the composition.

    METHOD FOR MANUFACTURING POLYROTAXANE
    108.
    发明公开
    METHOD FOR MANUFACTURING POLYROTAXANE 有权
    VERFAHREN ZUR HERSTELLUNG VON POLYROTAXAN

    公开(公告)号：EP2899221A1

    公开(公告)日：2015-07-29

    申请号：EP13839485.3

    申请日：2013-09-09

    Applicant: Sumitomo Seika Chemicals Co., Ltd. ,  Advanced Softmaterials Inc.

    Inventor： YAMASAKI Tomoaki ,  KIMURA Akira ,  OKAZAKI Hiroki ,  ZHAO Changming

    IPC: C08G65/329

    CPC classification number: C08G81/00 ,  C08B37/0015 ,  C08G65/332 ,  C08G65/33306 ,  C08G83/007 ,  C08L5/16 ,  C08L71/02

    Abstract: The present invention aims to provide a method for producing a polyrotaxane which enables industrially advantageous production of a polyrotaxane with a high inclusion rate.
    The present invention relates to a method for producing a polyrotaxane that includes a cyclodextrin; a compound having a repeating structural unit represented by the following formula (1), and threading through a cavity of the cyclodextrin in a skewered manner to be included in the cyclodextrin; and capping groups individually placed at each end of a molecule of the compound having a repeating structural unit represented by the formula (1) to prevent the cyclodextrin from separating, the method comprising: a step 1 of mixing the compound having a repeating structural unit represented by the formula (1) and the cyclodextrin in an aqueous medium to prepare an aqueous dispersion of pseudopolyrotaxan particles in which the compound having a repeating structural unit represented by the formula (1) is included in a cavity of a cyclodextrin molecule in a skewered manner; and a step 2 of mixing a triazine compound represented by the formula (2), a compound having at least one tertiary amino group, the aqueous dispersion of pseudopolyrotaxane particles prepared in the step 1, and a capping agent to introduce capping groups individually at each end of a molecule of the compound having a repeating structural unit represented by the formula (1) in the pseudopolyrotaxane particles,



    wherein, in the formula (2), R 1 and R 2 are each independently a C1-C4 alkyl group or a C6-C8 aryl group, and X represents a halogen atom.

    Abstract translation: 本发明的目的在于提供一种制造聚轮烷的方法，该聚轮烷能够以高夹杂率在工业上有利地制造聚轮烷。 本发明涉及一种生产包含环糊精的聚轮烷的方法; 具有由下式（1）表示的重复结构单元的化合物，并且以串行方式穿过环糊精的空腔包含在环糊精中; 和封端基团分别置于具有由式（1）表示的重复结构单元的化合物的每个末端，以防止环糊精分离，所述方法包括：步骤1，将具有重复结构单元的化合物 通过式（1）和环糊精在水性介质中制备其中具有由式（1）表示的重复结构单元的化合物以串联方式包含在环糊精分子的空腔中的假聚缩醛颗粒的水分散体 ; 和步骤2，将由式（2）表示的三嗪化合物，具有至少一个叔氨基的化合物，在步骤1中制备的假聚轮烷颗粒的水分散体和封端剂各自独立地引入封端基团 在所述假聚轮烷粒子中具有式（1）所示的重复结构单元的化合物的分子的末端，其中，在式（2）中，R 1和R 2各自独立地为C 1〜C 4烷基或C 6 -C8芳基，X表示卤素原子。

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