公开(公告)号：KR100115586B1

公开(公告)日：1997-05-24

申请号：KR1019930010109

申请日：1993-06-04

Applicant: 한국과학기술연구원

Inventor： 조정혁 ,  오창현 ,  류재천

IPC: C07C237/46 ,  C07C233/65 ,  C07C235/16

公开(公告)号：KR1019970001536B1

公开(公告)日：1997-02-11

申请号：KR1019930010109

申请日：1993-06-04

Applicant: 한국과학기술연구원

Inventor： 조정혁 ,  오창현 ,  류재천

IPC: C07C237/46 ,  C07C233/65 ,  C07C235/16

Abstract: Triiodide benzene derivative of general formula(I) is prepared by (1) reacting aniline derivative of general formula(II) with acetyl compound under organic based on the obtained aniline derivative of the general formula(III) preserved by a hydroxyl group, (2) reacting with M-hydroxy carboxylate of general formula(IV) preserved by acetyl group in organic solvent and adding guanidine of the same catalyst amount to acylating compound obtained from a general formula(V). In the formula, R1 and R2 is independently hydrogen, methyl and low-level alkyl group respectively.

Abstract translation: （I）的三碘化物苯衍生物通过以下方法制备：（1）将通式（II）的苯胺衍生物与有机基上得到的通式（III）的苯胺衍生物由羟基保护的（2） ）与通过乙酰基保护的通式（IV）的M-羟基羧酸酯在有机溶剂中反应，并将相同催化剂量的胍加入由通式（V）获得的酰化化合物中。 在该式中，R 1和R 2分别独立地为氢，甲基和低级烷基。