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    다공성 폴리올레핀 입자의 제조방법
    101.
    发明公开
    다공성 폴리올레핀 입자의 제조방법 无效
    制备多孔聚烯烃颗粒的方法

    公开(公告)号：KR1020010013416A

    公开(公告)日：2001-02-26

    申请号：KR1019997011417

    申请日：1998-06-02

    Applicant: 코닌클리즈케 디에스엠 엔.브이.

    Inventor： 쉬렌베르그루돌프루시엔 ,  스멜트하롤트잔 ,  드보스로엘로프프란시스쿠스게라르두스마리아

    IPC: C08J9/28

    CPC classification number: C08J9/28 ,  C08J2201/052 ,  C08J2201/0542 ,  C08J2323/02

    Abstract: The invention relates to a process for preparing porous polyolefin particles. The process according to the invention is characterized in that it comprises the following steps: 1) dissolving at least one crystallizable polyolefin in a solvent, in the absence of a nucleating agent; 2) dispersing the polyolefin solution obtained in a non-solvent in the presence of a surfactant, at a temperature that is higher than the crystallization temperature of the polyolefin in the polyolefin solution; 3) cooling the multi-phase system obtained with stirring, at a rate of between 0.05 and 10 °C/min to a temperature that lies below the crystallization temperature of the polymer in the polymer solution, so that firm polyolefin particles are formed; 4) separating the polyolefin particles; 5) drying the polyolefin particles. The invention also relates to a porous polyolefin particle with a high effective loadability and a narrow particle size distribution.

    Abstract translation: 本发明涉及一种制备多孔聚烯烃颗粒的方法。 根据本发明的方法的特征在于其包括以下步骤：1）在不存在成核剂的情况下将至少一种可结晶聚烯烃溶解在溶剂中; 2）在表面活性剂存在下，在高于聚烯烃溶液中的聚烯烃的结晶温度的温度下分散在非溶剂中获得的聚烯烃溶液; 3）以0.05〜10℃/分钟的速度搅拌得到的多相体系冷却到聚合物溶液中聚合物结晶温度以下的温度，形成坚固的聚烯烃粒子; 4）分离聚烯烃颗粒; 5）干燥聚烯烃颗粒。 本发明还涉及具有高有效负载能力和窄粒度分布的多孔聚烯烃颗粒。

    유전율이 매우 낮은 간층 유전체를 위한 나노 다공성중합체 필름
    103.
    发明公开
    유전율이 매우 낮은 간층 유전체를 위한 나노 다공성중합체 필름 无效
    用于具有非常低介电常数的中间层电介质的纳米聚合物膜

    公开(公告)号：KR1020000035596A

    公开(公告)日：2000-06-26

    申请号：KR1019990051635

    申请日：1999-11-19

    Applicant: 에어 프로덕츠 앤드 케미칼스, 인코오포레이티드

    Inventor： 오닐마크레오나드 ,  로베슨로이드맬론 ,  버고인쥬니어윌리엄프랭클린 ,  랭삼마이클

    IPC: C08J7/04 ,  B82B3/00

    CPC classification number: H01L21/02118 ,  C08J9/28 ,  C08J2201/0502 ,  C08J2201/0542 ,  H01B3/306 ,  H01B3/42 ,  H01B3/427 ,  H01B3/442 ,  H01L21/02203 ,  H01L21/02282 ,  H01L21/312 ,  H01L21/31695

    Abstract: PURPOSE: A nanoporous polymer film which overcomes the drawbacks of film thickness, dielectric constant, porosity, stability and adhesion of the prior art, and has low dielectric constant nanoporous thin films with good adhesion for use in dielectric layers for integrated circuits and various microelectronic devices, thereby allows the achievement of the high performance films and polymeric interlayer dielectrics in the reduced line dimensions contemplated by the electronic fabrication industry is provided. CONSTITUTION: A nanoporous polymer film is produced by following method comprising the steps of: providing a polymer in a solution with at least two solvents for the polymer, wherein a lowest boiling solvent and a highest boiling solvent have a difference in their respective boiling points of approximately 50°C or greater; forming a film of the polymer in solution with the at least two solvents on a substrate; removing a predominant amount of the lowest boiling solvent; contacting the film with a fluid which is a non-solvent for the polymer, but which is miscible with the at least two solvents; and forming a nanoporous film having average pore size in the film of less than 10 micrometer and low dielectric constant.

    Abstract translation: 目的：克服现有技术的膜厚度，介电常数，孔隙率，稳定性和粘附性的缺点的纳米多孔聚合物膜，并且具有用于集成电路和各种微电子器件的介电层中具有良好粘合性的低介电常数纳米多孔薄膜 ，从而允许实现由电子制造工业预期的减小的线尺寸的高性能膜和聚合物层间电介质。 构成：通过以下方法制备纳米多孔聚合物膜，其包括以下步骤：在溶液中提供聚合物至少两种用于聚合物的溶剂，其中最低沸点溶剂和最高沸点溶剂的沸点相差 大约50°C以上; 在溶液中用基材上的至少两种溶剂形成聚合物膜; 去除主要量的最低沸点溶剂; 使膜与用于聚合物的非溶剂的流体接触，但与至少两种溶剂可混溶; 并且在薄膜中形成平均孔径小于10微米和低介电常数的纳米孔膜。

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