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    PROCESS FOR PRODUCING HYDROXYALKYLATED POLYROTAXANE
    126.
    发明公开
    PROCESS FOR PRODUCING HYDROXYALKYLATED POLYROTAXANE 审中-公开
    VERFAHREN ZUR HERSTELLUNG VON羟基烷基聚氧乙烯

    公开(公告)号：EP2832750A1

    公开(公告)日：2015-02-04

    申请号：EP13770318.7

    申请日：2013-04-01

    Applicant: Ube Industries, Ltd. ,  Advanced Softmaterials Inc.

    Inventor： OOMORI, Kiyoshi ,  SADAIKE, Shinichiro ,  TSUGAWA, Mitsumasa ,  FUJIMOTO, Mikio ,  IWATA, Minoru ,  HAYASHI, Yuki

    IPC: C08B37/16 ,  C08G65/04

    CPC classification number: C08G83/007 ,  C08B37/0015 ,  C08L5/16 ,  C08L101/005 ,  C08L71/02

    Abstract: The invention provides an industrially advantageous method for the production of hydroxyalkylated polyrotaxanes. The method of producing hydroxyalkylated polyrotaxane includes reacting a polyrotaxane with a cyclic ether represented by Formula (1) in the presence of water and an organic base, wherein the polyrotaxane includes hydroxyl group-containing cyclic molecules, a linear molecule threaded through the cyclic molecules to form a clathrate, and blocking groups at both ends of the linear molecule to prevent the separation of the cyclic molecules from the linear molecule.

    Abstract translation: 本发明提供了用于生产羟烷基化聚轮烷的工业上有利的方法。 制备羟烷基化聚轮烷的方法包括在水和有机碱的存在下使聚轮烷与由式（1）表示的环醚反应，其中聚轮烷包括含羟基的环状分子，通过环状分子穿过的线性分子， 形成包合物，并且在线性分子的两端封闭基团以防止环状分子与线性分子的分离。

    PRODUCTION METHOD FOR POWDERED HYDROPHILIC MODIFIED POLYROTAXANE
    130.
    发明公开
    PRODUCTION METHOD FOR POWDERED HYDROPHILIC MODIFIED POLYROTAXANE 有权
    高效液相色谱法改性聚氧乙烯

    公开(公告)号：EP2687546A1

    公开(公告)日：2014-01-22

    申请号：EP11861040.1

    申请日：2011-12-05

    Applicant: Sumitomo Seika Chemicals Co., Ltd. ,  Advanced Softmaterials Inc.

    Inventor： YAMASAKI Tomoaki ,  OKAZAKI Shinya ,  OKAZAKI Hiroki ,  HAMAMOTO Shigeki ,  HAYASHI Yuki ,  IWATA Minoru

    IPC: C08B37/16 ,  C08G65/06 ,  C08J3/12

    CPC classification number: C08B37/0015 ,  C08G65/2606 ,  C08G65/3331 ,  C08G65/33396 ,  C08G2650/04 ,  C08J3/122 ,  C08J2305/16 ,  C08L71/02 ,  C08L5/16

    Abstract: The present invention aims to provide a method of producing a powdered hydrophilic modified polyrotaxane, which enables production of a powdered hydrophilic modified polyrotaxane excellent in storage stability in an industrially advantageous way. The present invention provides a method of producing a powdered hydrophilic modified polyrotaxane, comprising: a hydrophilic modification step of preparing a solution of a hydrophilic modified polyrotaxane by modifying all or part of hydroxy groups on a cyclodextrin of a polyrotaxane with hydrophilic modifying groups, the polyrotaxane containing the cyclodextrin, a polyethylene glycol included in the cavities of the cyclodextrin molecules in a skewered manner, and a capping group that is placed at each end of the polyethylene glycol and prevents dissociation of the cyclodextrin molecules from the polyethylene glycol; and a drying step of spraying the prepared solution of the hydrophilic modified polyrotaxane and drying the solution of the hydrophilic modified polyrotaxane in a heated gas stream.

    Abstract translation: 本发明的目的在于提供一种生产粉状亲水性改性聚轮烷的方法，该方法能够以工业上有利的方式制备具有优异的储存稳定性的粉末状亲水性改性聚轮烷。 本发明提供一种粉末状亲水性改性聚轮烷的制造方法，其特征在于，包括：亲水改性工序，其通过将聚轮烷的环糊精的全部或部分羟基改性为亲水性改性基来制备亲水改性聚轮烷的溶液，所述聚轮烷 包含环糊精，串联包含在环糊精分子的空腔中的聚乙二醇和置于聚乙二醇的每一端的封端基团，并防止环糊精分子与聚乙二醇分解; 以及干燥步骤，喷雾所述亲水改性聚轮烷的制备溶液，并将加热的气流中的亲水改性聚轮烷的溶液干燥。

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