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    POWDER COMPOSITION
    141.
    发明专利
    POWDER COMPOSITION 失效

    公开(公告)号：JPS62278535A

    公开(公告)日：1987-12-03

    申请号：JP12186686

    申请日：1986-05-27

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO ,  INOUE TAKEHISA ,  IZUMI NOBUMI

    IPC: C08J3/12 ,  G02F1/133 ,  G02F1/1339 ,  G09F9/30

    Abstract: PURPOSE:To distribute respective particles to a specified ratio and to decrease uneven spraying by using a mixture composed of epoxy spherical particles which contain a latent curing agent compatibly in the particles and are partially cured by an amine compd. and silica spherical particles. CONSTITUTION:The epoxy compd. contg. >=2 epoxy groups in the molecule is added to the latent curing agent. The amt. of the curing agent is usually specified to 0.05-1 equiv. per epoxy equiv. of an epoxy compd. and the epoxy compd. is partially cured by the amine curing agent to a spherical particle state. The epoxy spherical particles act as an adhesive component and are formed to have

    PARTICLE FOR COMPOUNDING TO COSMETIC OR QUASI-DRUG
    144.
    发明专利
    PARTICLE FOR COMPOUNDING TO COSMETIC OR QUASI-DRUG 失效

    公开(公告)号：JPS62198609A

    公开(公告)日：1987-09-02

    申请号：JP3901886

    申请日：1986-02-26

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO

    IPC: A61K8/19 ,  A61K8/00 ,  A61K8/04 ,  A61K8/73 ,  A61Q5/02 ,  A61Q17/04 ,  A61Q19/00 ,  C08J3/12

    Abstract: PURPOSE:To provide spherical particle of a polymer having amino group at side chain and modified by ionic adsorption with a compound having anionic group and useful for coloring, imparting of ultraviolet absorptivity, prevention of chapped skin, etc., as an additive for cosmetic, soap, shampoo, etc. CONSTITUTION:The objective spherical polymer particle has an average particle diameter of 0.1-100mum (preferably 0.2-70mum), contains amino group at side chain and modified by ionic adsorption with a compound having anionic group (e.g. sulfone group, carboxyl group, phenolic OH group, etc.) such as acidic dye, ultraviolet absorber, L-ascorbic acid, colorant for food, colorant for cosmetic, colorant for quasi-drug, etc. The polymer is chitosan or a copolymer containing acrylic monomer or aromatic vinyl monomer having amino group. A cosmetic having high bleed-out resistance can be produced by the use of the polymer particle. The particle exhibits a function of slow-releasing agent by contacting with an aqueous solution of NaCl, etc.

    PRODUCTION OF FINE SPHERICAL PARTICLE OF HEAT-RESISTANT EPOXY RESIN
    145.
    发明专利
    PRODUCTION OF FINE SPHERICAL PARTICLE OF HEAT-RESISTANT EPOXY RESIN 失效

    公开(公告)号：JPS62106921A

    公开(公告)日：1987-05-18

    申请号：JP24738385

    申请日：1985-11-05

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO

    IPC: A61K8/72 ,  A61K8/00 ,  A61K8/04 ,  A61K8/30 ,  A61K8/36 ,  A61K8/368 ,  A61K8/46 ,  A61K8/86 ,  A61Q1/02 ,  A61Q19/00 ,  C08G59/18 ,  C08G59/42 ,  C08G59/50 ,  C08J3/12

    Abstract: PURPOSE:To facilitate the formation of fine spherical particles of an epoxy resin improved in heat resistance and solvent resistance, by treating said particles cured with an amine curing agent with a polybasic acid. CONSTITUTION:Fine spherical particles of an epoxy resin, average particle diameter of 0.1-100mu, cured with an amine curing agent are treated with a polybasic acid. As processes for preparing said particles, (1) a process in which an uncured epoxy compound is cured after it is dispersed in an aqueous liquid and (2) a process in which an uncured epoxy compound and an amine curing agent are polymerized by static precipitation polymerization in a liquid polyol are particularly preferable from the viewpoint of the uniformity, sphericity, etc., of the particles. Above all, the process (1), especially, that in which an emulsion made by using a surfactant, etc., is used is preferable in respect of the rate of production. As the polybasic acids, mineral acids and compounds having carboxyl groups or sulfonic groups directly bonded to a benzene ring are used desirably.

    OPTICAL THIN FILM AND REFELCTION PREVENTIVE ARTICLE
    148.
    发明专利
    OPTICAL THIN FILM AND REFELCTION PREVENTIVE ARTICLE 失效

    公开(公告)号：JPH11133207A

    公开(公告)日：1999-05-21

    申请号：JP8130798

    申请日：1998-03-27

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO ,  NAKAKIMURA AKITOSHI ,  KONDO TETSUJI

    IPC: G02B1/11 ,  B32B27/00 ,  C08G59/30 ,  C08J5/18 ,  G02B1/10 ,  G02B1/111 ,  G02B1/14

    Abstract: PROBLEM TO BE SOLVED: To obtain the reflection preventive optical thin film easy in manufacture and superior in abrasion and scratching resistance by using a specified compound subjected to hardening treatment. SOLUTION: The reflection preventive optical thin film is made of the hardened compound represented by the formula in which Rf is an alkylene group containing F atoms; (a) is 0 or 1; and (b) is 0, 1, 2, or 3. Rf may be a straight car branched alkylene group, and a part or all of the H atoms are substituted by the F atoms. The preferable alkylene group to be used is a straight chain one from the point of easiness of manufacture and all the H atoms are, preferably, substituted by the F atoms in the case of perfluoroalkylene in order to obtain the optical thin film as low as possible in the reflective index. It is favorable from the point of the easiness of manufacture that (a) is 0 or 1, and if (b) exceeds 3, the hardness of the optical thin film tends to become insufficient.

    FLUORINE-CONTAINING COMPOUND AND OPTICAL THIN FILM AND ARTICLE CAPABLE OF PREVENTING REFLECTION
    149.
    发明专利
    FLUORINE-CONTAINING COMPOUND AND OPTICAL THIN FILM AND ARTICLE CAPABLE OF PREVENTING REFLECTION 失效

    公开(公告)号：JPH1135585A

    公开(公告)日：1999-02-09

    申请号：JP18955297

    申请日：1997-07-15

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO

    IPC: C07F7/12 ,  C07F7/18 ,  C08L63/00 ,  C09D5/00 ,  C09D183/04 ,  C09K3/00 ,  G02B1/11 ,  G02B1/111 ,  G02B1/14 ,  G02B1/16

    Abstract: PROBLEM TO BE SOLVED: To obtain a new fluorine-containing compound, having excellent thin- film forming properties, capable of forming a cured product having a low refractive index and a high hardness and excellent in scuff resistance and durability and useful for an optical thin film, an optical filter, etc. SOLUTION: This fluorine-containing compound is represented by formula I at least one of A1 to A4 is a group represented by formula II [X is OCH3 , OC2 H5 , OC3 H7 , OC4 H9 , Cl or Br; Y is CH3 , C2 H5 , C3 H7 or C4 H9 ; (b) is 1-6; (c) is 1-3] and the others are each H, (n) is 2-14}, e.g. 1,10-bis[2,3 -bis( N -[3 -(triethoxysilyl) propyl] carbamoyl} oxy)propyl] perfluorodecane. The compound represented by formula I is obtained by carrying out the urethanizing reaction of a compound represented by formula III with a compound represented by formula IV.

    OPTICAL THIN FILM, ANTIREFLECTIVE ARTICLE AND ANTIREFLECTION METHOD
    150.
    发明专利
    OPTICAL THIN FILM, ANTIREFLECTIVE ARTICLE AND ANTIREFLECTION METHOD 失效

    公开(公告)号：JPH112703A

    公开(公告)日：1999-01-06

    申请号：JP15542697

    申请日：1997-06-12

    Applicant: TORAY INDUSTRIES

    Inventor： OKA KOICHIRO

    IPC: G02B1/10 ,  B32B27/38 ,  B32B27/40 ,  C08G59/40 ,  C08J5/18 ,  G02B1/11 ,  G02B1/111 ,  G02B1/14

    Abstract: PROBLEM TO BE SOLVED: To obtain low reflective optical thin film which has a low refractive index, high surface hardness, has excellent flawing resistance and durability and is easily formable by curing a compsn. into which a specific crosslinkable fluorine-contg. compd. is incorporated, thereby forming the thin film. SOLUTION: The optical thin film is formed by curing the compsn. contg. the crosslinkable fluorine-contg. compd. obtd. by bringing a compd. having a perfluoro group and plural OH group within one molecule and a silane compd. having an isocyanate group and plural hydrolyzable groups bonded to silicon into urethanating reaction. The preferable crosslinkable fluorine-contg. compd. is exemplified by the compd. expressed by formula I. In the formula I, A1 and A2 denote the org. groups expressed by formula II and one thereof may be H; (n) is an integer from 2 to 14. In the formula II, X denotes -OCH3 , -OC2 H5 , -OC3 H7 , -OC4 H9 , -Cl ro -Br, Y denotes -CH3 , -OC2 H5 , -OC3 H7 , -OC4 H9 ; (b) denotes an integer from 1 to 6, (c) denotes an integer from 1 to 3.

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